“…This suggested that such loops might be formed, acting as hardening source in electron-irradiated commercial steels. Although quantitative data of interstitial components as matrix damage are quite scarce due to technical difficulty to identify them [40], such experimental efforts are needed to fully understand the cascade effects on hardening and embrittlement in commercial steels.…”
Section: Comparison Between Electron and Neutron Irradiationmentioning
“…This suggested that such loops might be formed, acting as hardening source in electron-irradiated commercial steels. Although quantitative data of interstitial components as matrix damage are quite scarce due to technical difficulty to identify them [40], such experimental efforts are needed to fully understand the cascade effects on hardening and embrittlement in commercial steels.…”
Section: Comparison Between Electron and Neutron Irradiationmentioning
“…The yield strength at 290°C is 570 MPa. In the previous studies, it was confirmed that well-defined solute clusters and dislocation loops form in this material under neutron, electron, and heavy-ion irradiations in unstressed condition [15][16][17][18][19].…”
Section: Specimen Preparation and Irradiation Conditionsmentioning
confidence: 52%
“…Observations were carried out using a TEM (Hitachi HF-3000) equipped with a field emission gun of 300 kV. Analysis of radiation induced defects was carried out at a depth of 600 nm in the specimens using a weak-beam technique; details of this had been described in previously [17].…”
“…Observations were carried out using a TEM (Hitachi HF-3000) equipped with a field emission gun of 300 kV. Analysis of radiation-induced defects was carried out at a depth of 300 nm in the specimens using a weak-beam technique; details have been described in the previous study [4].…”
Section: Measurementsmentioning
confidence: 99%
“…More experimental data obtained by well-controlled irradiation at a specific dose rate and temperature are needed to understand the effects of dose rate change during irradiation on the microstructure change. Ion irradiation experiments are one of the best methods for carrying out a well-controlled irradiation, and they have been applied to the investigation of radiation embrittlement in previous studies [4][5][6].…”
Iron-ion irradiations were carried out for 0.09wt%Cu A533B steel specimens at 2908C to investigate effects of dose rate change during irradiation; the irradiations consisted of the base irradiation (with an unchanged dose rate) and an additional one with changed dose rates from 1 to 50 times that of the base one. Nano-indentation hardness measurements showed that the increase in hardness was higher for lower dose rate of the base irradiation. A similar trend was identified during the additional irradiation. Transmission electron microscope (TEM) and three-dimensional atom probe (3DAP) analyses were carried out for the quantitative characterization of defect features. Mn/Ni/Si/Cu-enriched clusters and dislocation loops were observed in all specimens. The increase in hardness mainly depended on the formation of the solute atom clusters. The square root of the volume fraction of the solute atom clusters provided a good correlation with the increase in hardness. The effects of dose rate and dose rate change during irradiation were explained by the formation of solute atom clusters.
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