Chemical composition of essential oils from aerial parts of <i>Cinnamomum malabatrum</i> (Burman f.) Bercht &amp; Presl.

Leela, N. K.; Vipin, T.M.; Shafeekh, K. M.; Priyanka, V.; Rema, J.

doi:10.1002/ffj.1910

Cited by 21 publications

(13 citation statements)

References 12 publications

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“…Up to date, TLC [24], HPLC [5,[25][26][27], GC [4,28,29] and GC-MS [30][31][32][33] have been developed for analysis of different species of Cinnamomum. However, these methods focused on the qualitative analysis [25,27,[29][30][31][32] or quantitative determination of few components [26,28,33], due to the lack of reference compounds. In addition, sample preparation is the crucial first step in the analysis of herbs and roughly accounts for approximately 30% of the analytical error [34].…”

Section: Introductionmentioning

confidence: 99%

Pressurized liquid extraction and GC‐MS analysis for simultaneous determination of seven components in Cinnamomum cassia and the effect of sample preparation

Huang

Yang

et al. 2010

J of Separation Science

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A pressurized liquid extraction and GC-MS method was developed for simultaneous quantitative determination of the seven components, including cinnamaldehyde, copaene, cinnamic acid, coumarin, 2-methoxycinnamaldehyde, 2-methoxycinnamic acid and safrole in Cinnamomum cassia. The results showed that methanol and ethanol was not available for extraction of cinnamaldehyde and 2-methoxycinnamaldehyde due to aldol reaction. The developed method was validated to be sensitive, accurate and simple, and was successfully employed for the analysis of 15 samples of C. cassia. The contents of the investigated components were significantly variant and cinnamaldehyde is the most abundant compound, but safrole was not detected in all samples.

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Section: Introductionmentioning

confidence: 99%

Pressurized liquid extraction and GC‐MS analysis for simultaneous determination of seven components in Cinnamomum cassia and the effect of sample preparation

Huang

Yang

et al. 2010

J of Separation Science

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“…Many of the species of Cinnamomum have medicinal and spice value, C. verum being the most important. Due to its economic importance and medicinal values, the genus has attracted the attention of phytochemists, and several terpenes, flavonoids, alkaloids and aliphatic compounds have been isolated (1)(2)(3)(4)(5)(6)(7). Even though several species have been subjected to phytochemical studies, there are some endemic species that are not explored for their chemical constituents.…”

Section: Introductionmentioning

confidence: 99%

Cinnamomum citriodorumThw. – new source of citronellol

Leela¹,

Vipin²,

Priyanka³

et al. 2012

Journal of Essential Oil Research

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The essential oil composition of Cinnamomum citriodorum leaves and petioles was determined by gas chromatography (GC) and GC-mass spectrometry (GC-MS) analysis. Leaf and petioles yielded 0.11% and 0.42% essential oil respectively. In leaf oil, twenty-seven constituents representing 97.2% of the oil were identified. Major components of the oil were citronellol (66.5-71.1%), citronellal (10.8-10.9%) and trans-geraniol (5.9-6.5%). In the oil from the petiole, thirty-eight compounds contributing 91.3% of the oil were identified, of which citronellol (36.2-38.3%), citronellal (9.9-15.4%) and α-copaene (8.7-10.3%) were the chief constituents. Although both oils were dominated by monoterpene alcohols, the oil from the petiole contained a higher level of sesquiterpenes (26.3-36.2%) compared with the leaf oil (5.0-9.9%).

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“…Moreover, the composition of cinnamon oil differs from the different parts of the cinnamon tree. For example, the bark oil is rich in CA, 2‐MCA, and CAc, etc., whereas the leaves and fruits of cinnamon mainly produce the volatile oil, in which CAc is the major constituent, accompanied by CA . The purified components extracted from these oils can be applied in many fields.…”

Section: Introductionmentioning

confidence: 99%

“…For example, the bark oil is rich in CA, 2-MCA, and CAc, etc., [4][5][6] whereas the leaves and fruits of cinnamon mainly produce the volatile oil, in which CAc is the major constituent, accompanied by CA. [7][8][9] The purified components extracted from these oils can be applied in many fields. Among these components, CA and CAc are the most important.…”

Section: Introductionmentioning

confidence: 99%

Facile separation of cinnamyl acetate and cinnamaldehyde based on host–guest complexation with β‐cyclodextrin

Chai

Zheng

et al. 2018

Flavour & Fragrance J

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A selective inclusion of cinnamyl acetate (CAc) is observed during the complexation of CAc and cinnamaldehyde (CA) with β‐cyclodextrin (β‐CD) in aqueous solution. To demonstrate the potential application of β‐CD for the separation of CAc and CA, the preferential affinity of β‐CD for CAc over CA was studied from conformational and thermodynamic points of view. Determination of the complexation geometries, performed by 1H and 2D (XRD), confirmed the inclusion capacity of the β‐CD cavity for CAc and CA. From the stability constants measured by ultraviolet‐visible (UV–Vis) spectroscopy and thermodynamic parameters measured by isothermal titration microcalorimetry, it was found that compared to CA, hydrophobic and hydrogen bonding interactions jointly promote CAc to form a more stable β‐CD binding complex with 1:1 stoichiometry. Furthermore, the higher binding affinity of β‐CD for CAc (over CA) was investigated theoretically in terms of binding energy and inclusion geometries. The separation of the equimolar CAc–CA mixture was achieved by inclusion complexation in β‐CD aqueous solution. The effects of the experimental conditions, such as the polarity of the solvent and guest/host molar ratio, on separation performance were investigated. Under the optimized conditions, the selective inclusion procedure exhibited a CAc/CA separation factor of 3.5, which remained stable after five cycles, indicating that β‐CD is a highly reusable host material.

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Chemical composition of essential oils from aerial parts of Cinnamomum malabatrum (Burman f.) Bercht & Presl.

Cited by 21 publications

References 12 publications

Pressurized liquid extraction and GC‐MS analysis for simultaneous determination of seven components in Cinnamomum cassia and the effect of sample preparation

Pressurized liquid extraction and GC‐MS analysis for simultaneous determination of seven components in Cinnamomum cassia and the effect of sample preparation

Cinnamomum citriodorumThw. – new source of citronellol

Facile separation of cinnamyl acetate and cinnamaldehyde based on host–guest complexation with β‐cyclodextrin

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