Chemically modified polyurethane-SiO2/TiO2 hybrid composite film and its reusability for photocatalytic degradation of Acid Black 1 (AB 1) under UV light
“…They had rough surfaces compared to the SiO 2 spheres because of the amount of TiO 2 nanoparticles deposited on the SiO 2 spheres which was only four atomic percent as confirmed by EDS [31]. The TiO 2 nanoparticles coating the SiO 2 spheres produced the advantage of increasing the active surface area, which helped to improve the photocatalytic activity.…”
Section: Characterizations Of Catalystmentioning
confidence: 77%
“…The SiO 2 spheres and SiO 2 @TiO 2 composite spheres were synthesized using the same procedure as our previous study [31]. The synthesis process is as follows: 2 mL TEOS, 0.6 mL dodecane, 10 mL anhydrous ethanol, 2 mL water, 0.4 mL ammonia solution, and 6 mL anhydrous ethanol were added in sequence to form a mixture that was stirred for 2 h at room temperature.…”
Section: Synthesis Of Sio 2 Spheres and Sio 2 @Tio 2 Composite Spheresmentioning
confidence: 99%
“…3 shows FE-SEM images of (a) 1 wt% Ag-SiO 2 @TiO 2 , (b) 2 wt% Ag-SiO 2 @TiO 2 , and (c) 3 wt% Ag-SiO 2 @TiO 2 composite spheres and the (d) EDX spectrum of the 3 wt% Ag-SiO 2 @TiO 2 spheres. The sizes of the SiO 2 spheres and SiO 2 @TiO 2 composite spheres are 310 and 320 nm, respectively [31]. A very thin layer of TiO 2 nanoparticles was deposited on the surface of the SiO 2 spheres.…”
“…They had rough surfaces compared to the SiO 2 spheres because of the amount of TiO 2 nanoparticles deposited on the SiO 2 spheres which was only four atomic percent as confirmed by EDS [31]. The TiO 2 nanoparticles coating the SiO 2 spheres produced the advantage of increasing the active surface area, which helped to improve the photocatalytic activity.…”
Section: Characterizations Of Catalystmentioning
confidence: 77%
“…The SiO 2 spheres and SiO 2 @TiO 2 composite spheres were synthesized using the same procedure as our previous study [31]. The synthesis process is as follows: 2 mL TEOS, 0.6 mL dodecane, 10 mL anhydrous ethanol, 2 mL water, 0.4 mL ammonia solution, and 6 mL anhydrous ethanol were added in sequence to form a mixture that was stirred for 2 h at room temperature.…”
Section: Synthesis Of Sio 2 Spheres and Sio 2 @Tio 2 Composite Spheresmentioning
confidence: 99%
“…3 shows FE-SEM images of (a) 1 wt% Ag-SiO 2 @TiO 2 , (b) 2 wt% Ag-SiO 2 @TiO 2 , and (c) 3 wt% Ag-SiO 2 @TiO 2 composite spheres and the (d) EDX spectrum of the 3 wt% Ag-SiO 2 @TiO 2 spheres. The sizes of the SiO 2 spheres and SiO 2 @TiO 2 composite spheres are 310 and 320 nm, respectively [31]. A very thin layer of TiO 2 nanoparticles was deposited on the surface of the SiO 2 spheres.…”
“…6F). Table 1 shows that the BET surface area of the synthesized TiO 2 /PU (110.4 m 2 /g) was not only greatly higher than that of the PU (30.46 m 2 /g) but also much higher than the surface area of commercial TiO 2 powder (60 m 2 /g) [23,47]. This result indicates that the immobilization of TiO 2 onto surface of honeycomb-structure PU greatly increased the surface area of TiO 2 .…”
“…However, during casting of the membranes, the crystalline peaks of the chitosan powder changed to an amorphous structure for the CA membrane. The broad SiO 2 peak was also observed at 2θ ¼ 221, which is commonly observed for SiO 2 [25][26][27].…”
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