1976
DOI: 10.1002/chin.197637254
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ChemInform Abstract: DEHYDROGENATION OF N‐SECONDARY CYCLIC AMINALS AND ACYLAMINALS

Abstract: Die N‐1‐terti= ären Chinazolinone (I) lassen sich mit dem Quecksilber(II)?AeDTA‐Komplex zu (II) dehydrieren.

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“…By comparison of the NMR and MS data with those published in the literatures, 26 known compounds were determined to be aurantiomide C (11) [14], cyclopenin (12) [19], (−)-cyclopenol ( 13) [20], (3S)-1,4-benzodiazepine-2,5-diones ( 14) [21], 3-benzylidene-3,4dihydro-4-methyl-lH-l,4-benzodiazepine-2,5-dione ( 15) [22], 3-methyl-3,4-dihydroquinazo line-4-one ( 16) [23], 1,2-dihydro-2,3-dimethyl4(3H)quinazolinone ( 17) [24], N,N'-1,2-pheny lenebis-acetamide ( 18) [25], aconicarpyrazine B ( 19) [26], pyroglutamylleucinmethylester (20) 29) [32], methyl phydroxybenzeneacetate (30) [33], 2-hydroxy phenyl acetic acid (31) [34], methyl homogentisate (32) [35], 5-hydroxymethyl-furaldehyde (33) [36], leptosphaerone A (34) [37], 3-methyl-2-penten-5-olide (35) [38], and (R)-mevalonolactone (36) [39].…”
Section: Resultsmentioning
confidence: 99%
“…By comparison of the NMR and MS data with those published in the literatures, 26 known compounds were determined to be aurantiomide C (11) [14], cyclopenin (12) [19], (−)-cyclopenol ( 13) [20], (3S)-1,4-benzodiazepine-2,5-diones ( 14) [21], 3-benzylidene-3,4dihydro-4-methyl-lH-l,4-benzodiazepine-2,5-dione ( 15) [22], 3-methyl-3,4-dihydroquinazo line-4-one ( 16) [23], 1,2-dihydro-2,3-dimethyl4(3H)quinazolinone ( 17) [24], N,N'-1,2-pheny lenebis-acetamide ( 18) [25], aconicarpyrazine B ( 19) [26], pyroglutamylleucinmethylester (20) 29) [32], methyl phydroxybenzeneacetate (30) [33], 2-hydroxy phenyl acetic acid (31) [34], methyl homogentisate (32) [35], 5-hydroxymethyl-furaldehyde (33) [36], leptosphaerone A (34) [37], 3-methyl-2-penten-5-olide (35) [38], and (R)-mevalonolactone (36) [39].…”
Section: Resultsmentioning
confidence: 99%