ChemInform Abstract: SYNTHESIS OF AMINOMETHYL DERIVATIVES OF 2‐HYDROXY‐5‐TERT‐ALKYLTHIOPHENOLS AND THEIR CLEAVAGE BY THIOLS

Kuliev, A. M.; Aliev, Sh. R.; Mamedov, F. N.; Movsumzade, M. M.

doi:10.1002/chin.197624210

Cited by 5 publications

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“…DP were synthesized according to the procedure [37]. The reagent was characterized by taking the elemental analysis, NMR and IR spectra [38] [39] [40].…”

Section: Resultsmentioning

confidence: 99%

Analytical Application of Ion Associates of Molybdenum with Dithiolphenols and Aminophenols

Kuliev¹,

Verdizade²,

Aliev³

et al. 2019

MSCE

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The mixed-ligand complexes of molybdenum(VI) with dithiolphenols (DP) {2,6-dithiol-4-methylphenol (DTMP), 2,6-dithiol-4-ethylphenol (DTEP) and 2,6-dithiol-4-tert-butylphenol (DTBP)} in the presence of hydrophobic amines have been investigated by spectrophotometric method. The condition of complexing and extraction, physical-chemical and analytical characteristics of this complex have been found. As hydrophobic amine 2(N, N-dimethylaminomethyl)-4-methylrphenol (АP 1) and 2(N, N-dimethylaminomethyl)-4-xlor-phenol (AP 2), 2 (N, N-dimethylaminomethyl)-4-brom-phenol (AP 3) were used. It has been found that mixed-ligand complex was formed in weakly acidic medium (pH 4.1-5.9). The maximum analytical signal when complexing Mo(V) is observed at 516-534 nm. The calculated molar absorption (ε max) belongs to the range (4.16-5.35) × 10 4. The Beer's law was applicable in the range of 0.3-22 µg/ml. The extraction photometric methods of the molybdenum determination were processed. The influence of diverse ions on determination of molybdenum has been studied. The proposed method was applied successfully to determine amount of molybdenum in steel and in soil.

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“…DP were synthesized according to the procedure [37]. The reagent was characterized by taking the elemental analysis, NMR and IR spectra [38] [39] [40].…”

Section: Resultsmentioning

confidence: 99%

Analytical Application of Ion Associates of Molybdenum with Dithiolphenols and Aminophenols

Kuliev¹,

Verdizade²,

Aliev³

et al. 2019

MSCE

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“…HTPh was synthesized according to the procedure [19]. Chloroform solutions of HTPh (0.01 mol L -1 ) and DPG (0.025 mol L -1 ) were used.…”

Section: Methodsmentioning

confidence: 99%

Research Into Complex Formation of Cobalt(ii) and Nickel (Ii) With 2-Hydroxy-5-Nitrothiophenol and Diphenylguanidine

Aliyev¹,

Исмайлова²,

Ibrahimova³

et al. 2018

Chemical Problems

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“…Characterization of the Reagent: DTMP were synthesized according to the procedure 42 . The reagent was characterized by taking the elemental analysis, NMR and IR spectra [43][44][45] .…”

Section: Methodsmentioning

confidence: 99%

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2017

IJPSR

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ChemInform Abstract: SYNTHESIS OF AMINOMETHYL DERIVATIVES OF 2‐HYDROXY‐5‐TERT‐ALKYLTHIOPHENOLS AND THEIR CLEAVAGE BY THIOLS

Abstract: Die Hydroxythiophenole (I) reagieren in wäßriger Lösung bei 20 ‐25°C mit Formaldehyd und Diäthylamin (analog auch Dimethyl‐, Dibutylamin, Piperidin, Morpholin) unter Bildung der Aminomethyl‐ Derivate (II).

Cited by 5 publications

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Analytical Application of Ion Associates of Molybdenum with Dithiolphenols and Aminophenols

Analytical Application of Ion Associates of Molybdenum with Dithiolphenols and Aminophenols

Research Into Complex Formation of Cobalt(ii) and Nickel (Ii) With 2-Hydroxy-5-Nitrothiophenol and Diphenylguanidine

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