It was demonstrated recently, that in transpiration cooled environments, the plenum pressure is sensitive to the surface heat flux. The Pressure Based Non-Integer System Identification (NISIp) method was found to be useful for the identification of pressure impulse responses of such systems. Using an identified system, an unknown surface heat flux can be reconstructed by measurement of the plenum pressure and deconvolution with the found pressure impulse response. Since a heat flux measurement at transpiration cooled surfaces is of fundamental interest in many applications of high-speed vehicles and propulsion systems, this methodology is intended to be further developed towards a heat flux sensor. A review of the methodology, the experimental setup and the results of first heat flux measurements in the plasma wind tunnel PWK4 at the Institute of Space Systems, Stuttgart are presented in this paper. Surface heat flux profiles for different coolant mass flow rates have been successfully determined using plenum pressure data.