Corrections for systematic errors from analog integration in controlled-potential coulometry

Frazzini, Thomas L.; Holland, Michael; Weiss, J.R.; Pietri, C.E.

doi:10.1021/ac50063a029

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Cited by 5 publications

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“…Calibration was accomplished by using the potentiostat to apply a precise voltage to a standard 99.996resistor for a period of 400-500 s measured by a quartz millisecond clock. This voltage, and also the resulting integrator output voltage, was measured with a Hewlett-Packard Model 3455A digital voltmeter, and corrections for capacitor leakage were applied as described by Frazzini et al (7). The electrical calibration was the basis for calculating the iodate content of the samples.…”

Section: Methodsmentioning

confidence: 99%