2015
DOI: 10.1039/c5ce01128k
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Crystal structure analysis of molecular dynamics using synchrotron X-rays

Abstract: Recent developments of X-ray crystallography using synchrotron X-rays have made it an improved analytical approach compared with the previously used temporally and spatially averaged observations in an analyte crystal. The short-pulse character of synchrotron X-rays enables conduction of a time-resolved X-ray experiment to observe the temporal three-dimensional dynamics in a crystal. This experimental technique is useful for studies regarding photo-induced phenomena. Additionally, high intensity X-rays from a … Show more

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Cited by 8 publications
(4 citation statements)
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“…This allows full control of the sample and easy measurement automation. Appropriate instrumentation solutions have already been implemented at synchrotron sources (Chen et al, 2014;Graber et al, 2011;Nowell et al, 2012;Hoshino et al, 2015) and have enabled steady-state and pump-probe photocrystallographic experiments. Nevertheless, since synchrotron time is limited, in cases where a very high X-ray flux is not necessary, it can be helpful to use a home laboratory setup.…”
Section: Introductionmentioning
confidence: 99%
“…This allows full control of the sample and easy measurement automation. Appropriate instrumentation solutions have already been implemented at synchrotron sources (Chen et al, 2014;Graber et al, 2011;Nowell et al, 2012;Hoshino et al, 2015) and have enabled steady-state and pump-probe photocrystallographic experiments. Nevertheless, since synchrotron time is limited, in cases where a very high X-ray flux is not necessary, it can be helpful to use a home laboratory setup.…”
Section: Introductionmentioning
confidence: 99%
“…It was put into operation in early 2000 s. The total number of beamlines open to user services is 13 and several large-scale instrumentation upgrade programs are currently underway. The 'Belok' beamline is one of the 1st priority beamlines, commissioned in 2004 [33].…”
Section: General Description Of the 'Belok' Beamline At The Kurchatovmentioning
confidence: 99%
“…The use of synchrotron radiation provides some evident advantages, such as the possibility of studying tiny and imperfect crystals, reducing mean data acquisition time, collecting diffraction data to high 2θ scattering angles to improve the quality of electron density distribution maps, etc. Real-time crystallographic studies of dynamical processes in crystals, such as solid-state reactions, phase transitions, conformational changes upon photoexcitation, become increasingly important [12][13][14][15].…”
Section: Introductionmentioning
confidence: 99%
“…For instance, X-ray diffractometry, which is essentially a method for analyzing ordered structures, does not generally have the temporal resolution required to track the PCMT process. 22 Luminescence is a promising property for the in situ observations of phase transitions because it allows the real-time, high-sensitivity detection of the emissive part in a bulk material. 1,[23][24][25] Microscopic visualizations of the crystallization process based on time-course luminescence has been reported previously.…”
mentioning
confidence: 99%