2010
DOI: 10.1524/ncrs.2010.0157
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Crystal structure of (Z)-1-(2,4-dinitrophenyl)-2-(3-methyl-2- nitrocyclohex-2-enylidene)hydrazine, C13H13N5O6

Abstract: C 13 H 13 N 5 O 6 ,monoclinic, P12 1 /c1(no. 14), a =14.501(2) Å, b =6.362(1) Å, c =17.166(2) Å, b =110.913(9)°, Source of materialThe stock solutions was prepared by dissolving 0.5 mmol (Z)-1-(2,4-dinitrophenyl)-2-(3-methylcyclohex-2-enylidene)-hydrazine in 100 ml dry CH 2 Cl 2 .NOwas produced by the reaction of 1mol H2SO4 solution with saturated NaNO2 aqueous solution. The former was added to the latter, which was stirred under argon atmosphere. NO was carried by argon and purified by passing it through aser… Show more

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“…The molecular structure of 2l in the solid state was confirmed by X-ray crystal structure analysis (Figure ) . Interestingly, the length of the newly formed C–N bond was only 1.341 Å, which was significantly shorter than a traditional C–N single bond but compared well to the bond length of a C–N double bond …”
mentioning
confidence: 99%
“…The molecular structure of 2l in the solid state was confirmed by X-ray crystal structure analysis (Figure ) . Interestingly, the length of the newly formed C–N bond was only 1.341 Å, which was significantly shorter than a traditional C–N single bond but compared well to the bond length of a C–N double bond …”
mentioning
confidence: 99%