Cu2O/CuO@mont K 10 promoted one-pot synthesis of 1,2,3-triazoles through azide-alkyne cycloaddition reaction

Clay based heterogeneous catalysts for carbon–nitrogen bond formation: a review

“…Pathak and his research group 114 published a work of azide–alkyne cycloaddition reaction for the synthesis of 1,2,3-triazoles 99 using a Cu 2 O/CuO@MK-10 heterogeneous catalyst. A simple one-pot click chemistry method was used for synthesizing 1,2,3-triazole.…”

A New Insight Into The Huisgen Reaction: Heterogeneous Copper Catalyzed Azide‐Alkyne Cycloaddition for the Synthesis of 1,4‐Disubstituted Triazole (From 2018–2023)

“…Pathak and his co‐worker synthesized a novel nanohybrid material, composed of Cu 2 O/CuO nanoparticles supported on Mont K 10 clay, which has been successfully synthesized using a biogenic approach that relies on an aqueous extract of Tulsi (Ocimum sanctum) leaves as both a reducing and stabilizing agent [74] . The presence of organic constituents in the leaves, including alkaloids, terpenoids, polyphenols, etc., plays a crucial role in anchoring the nanoparticles onto the Mont K 10 clay matrix.…”

“…Pathak and his co-worker synthesized a novel nanohybrid material, composed of Cu 2 O/CuO nanoparticles supported on Mont K 10 clay, which has been successfully synthesized using a biogenic approach that relies on an aqueous extract of Tulsi (Ocimum sanctum) leaves as both a reducing and stabilizing agent. [74] The presence of organic constituents in the leaves, including alkaloids, terpenoids, polyphenols, etc., plays a crucial role in anchoring the nanoparticles onto the Mont K 10 clay matrix. The FT-IR spectra of Mont K 10 and Cu 2 O/CuO@mont K 10 show characteristic peaks, with Mont K 10 exhibiting peaks at 3435 cm À 1 and 1636 cm À 1 attributed to OÀ H stretching and bending vibrations of free water molecules, and a peak at 1090 cm À 1 due to the asymmetric stretching vibration of siloxane (SiÀ OÀ Si) moiety.…”