“…By acid activation of raw Maghnite with a 0.25M H 2 SO 4 solution, there is a complete cationic exchange of Maghnite by protons, without destroying its structure. 39 The Mag-H + obtained is widely used in the ring-opening polymerizations 26,[40][41][42][43][44][45] , also in the synthesis of bis-macromonomers 6,7,46 , and it has many advantages such as very low purchase price compared to other catalysts and the easy removal of the reaction mixture, regenerated by heating to a temperature above 373 K. 40,41 In our work, we were interested in using a new method for a green synthesis of telechelic PGPTMS with acetate and methacrylate end groups, in bulk, using one step, by cationic ring-opening polymerization of 3-glycidoxypropyltrimethoxysilane (GPTMS), in the presence of acetic anhydride (AA) and methacrylic anhydride (MA), using a green catalyst Mag-H + without spending energy. The best results in term of activation and yield of the product are determined using the kinetic study on the evolution of the synthesis reaction.…”