Abstract. In this paper, the microstructure, phase structure, hardness and micro-hardness of Co 37+x Ni 34-x Al 29 (x=0,1,2,3) alloys studied by optical micrograph, X-ray diffraction, hardness test and compressive test. The results show that the β phase and γ phase coexist within Co 37+x Ni 34-x Al 29 (x=0,1,2,3) alloys. The γ phase at the grain boundary became coarse with Co content increasing. Meanwhile, the grain size of alloy decreases with Co content increasing. The hardness of Co-Ni-Al alloy decrease first and then increase with Co content rising. The micro-hardness of γ and β phase in Co 38 Ni 33 Al 29 alloy is 454 HV and 713 HV, respectively.