Determination of neodymium, samarium and europium

Komori, Takuji; Tamura, Shuzo; Ouchi, Misao; Gunji, Katsubumi; Hashitani, Hiroshi; Yoshida, Hiroyuki

doi:10.2116/bunsekikagaku.13.32

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1968

1969

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“…Aziridines, for example, may be prepared by the alkali treatment of a fl-chloroamine salt (2,4). Komori et al (5,6) prepared various chlorinated fatty amine hydrochlorides by the free radical chlorination of saturated amine hydrochlorides. The chlorination products contained from 1 to 4 chlorine atoms per fatty chain, but the free, chlorine-containing amines were not described.…”

Section: Introductionmentioning

confidence: 99%

Chlorinated alcohols: III. 9,10‐Dichlorostearylamine

Grimm

Stirton

Weil

1968

J Americ Oil Chem Soc

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9,10-Dichlorostearylamine was prepared by the hydrogenation of 9,10-dichlorostearonitrile, catalyzed by Rh/C, and by the chlorination of oleylamine hydrochloride. The dichloro amine was surprisingly heat-stable and could be purified by molecular distillation at 170 C (0.1 ram). Also described are the preparations of 9,10dichlorostearoyl chloride, 9,10-dichlorostearamide and 9,10-diehlorostearonitrile. The chlorination of oleonitrile is not a simple reaction and the 9,10-dichlorostearonitrile was best prepared by dehydration of the amide.

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Section: Introductionmentioning

confidence: 99%