Determination of traces of hydrogen, nitrogen and oxygen in aqueous solutions by gas chromatography

Polyaddition of Dithiol Compounds to Diethynyl Compounds: Kinetics of the Model Addition Reaction of Thiophenol to Ethynylbenzene

“…Nitrogen gas was purified as shown in the previous paper 14 and then through a glass column containing molecular sieve 3A at near liquid nitrogen temperature, since the molecular sieve 3A absorbs oxygen at low temperature. 15 …”

Gas chromatographic determination of dissolved hydrogen and oxygen in photolysis of water

“…In an attempt to observe trace quantities of H2 and 02 which might be evolved during the photolysis of glass supported monolayer assemblies of surfactant derivatives of tris(2,2'-bipyridine)ruthenium(II) (2), a simple chromatographic method has been utilized and is reported here. Determination of traces of H2, N2, and 02 in aqueous solutions by vapor phase chromatography has been reviewed by Tolk and co-workers (4). In the present method, the aqueous solution is injected directly onto a chromatographic column filled with molecular sieves and the eluting H2 and 02 monitored by a standard thermal conductivity detector.…”