Abstract-The aim of this study is the investigation of electrohydrolysis treatment process for olive mill wastewater in terms of pollutants removal and hydrogen production. For this purpose, Different voltages including 4, 6 and 8 V DC were tested for 3 hours. 8 V DC for 3 hours was found to be as the most effective condition. At this optimum voltage, different time periods were also investigated. At 8 V, significant pollutant removal efficiencies were obtained. 68% turbidity, 70% TSS, 52% COD and 19% sCOD removal efficiencies were achieved. Volume of produced gas was 1500±10 ml and hydrogen percent was determined as 85%. Hydrogen production along with pollutant removal is one of the advantages of electrohydrolysis. Therefore, electrohydrolysis can be proposed as a feasible alternative treatment step for wastewaters which is characterized by high organic matter and also suspended matter.