Development and validation of an air monitoring method for 1,3-dichloropropene, trans-1,2,3-trichloropropene, cis-1,2,3-trichloropropene, 1,1,2,3-tetrachloropropene, 2,3,3-trichloro-2-propen-1-ol, and 1,1,2,2,3-pentachloropropane

Leiber, Mark A.; Berk, Howard C.

doi:10.1021/ac00276a035

Anal. Chem.

1984

DOI: 10.1021/ac00276a035

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Development and validation of an air monitoring method for 1,3-dichloropropene, trans-1,2,3-trichloropropene, cis-1,2,3-trichloropropene, 1,1,2,3-tetrachloropropene, 2,3,3-trichloro-2-propen-1-ol, and 1,1,2,2,3-pentachloropropane

Mark A. Leiber¹,

Howard C. Berk²

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Cited by 9 publications

References 18 publications

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Adsorption/Thermal Desorption with Tenax‐GC for the Collection and Analysis of Polycyclic Aromatic Hydrocarbons and Chlorinated Compounds

Sye

Chang

1989

J Chinese Chemical Soc

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A system for the determination of polycyclic aromatic hydrocarbons(PAHs) and chlorinated compounds. in air by means of adsorption/thermal desorption(AID) with small bed volume (O.lg) Tenax cartridges, followed bycryogenic trap in a V-shaped stainless , steel tube with liquid nitrogen as an appropriate concentration method prior to capillary gas chromatography is described, Recoveries were determined .for the complete ATO method. Desorption recoveries near 100% were found for a variety of chlorinated compounds and polycyclic aromatic bydrocarbons.

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Adsorption/Thermal Desorption with Tenax‐GC for the Collection and Analysis of Polycyclic Aromatic Hydrocarbons and Chlorinated Compounds

Sye

Chang

1989

J Chinese Chemical Soc

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Determination of soil fumigants in air using tandem capillary gas chromatography after charcoal trapping

Tuinstra¹,

Traag²,

Roos³

1988

J. High Resol. Chromatogr.

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is acknowledged for supplying the plasma samples tested. References[l] B. Hedback and L. S. Hermann, Acta Med. Scand. suppl. 681 (1984) 129-134. [2] M. Schomerus, B. Spiegelhalder, B. Stieren, and M. Eichelbaum, Cardiovasc. Res. 10 (1976) 605-61 2. G. Neugebauer, Cardiovasc. Res. 12 (1978) 247-254 G. M. Thomson and L. K. Pannell, J. Anal. Toxicol. 5 (1981) [3] [4] 105-1 09. [5] S. R. Harapat and R. . 70 (1981) V. K. Piotrovskii, D. 0. Ruminatsev, and V. 1. Metelitsa, J. Chromatogr. 275 (1983) 95-200. P. A. Kapur, T. L. Aw, and E. Watson, J. Chrornatogr. 337 222 (1981) 507-51 1. 800-80 1 .(1 985) 160-1 65. SummarySoil fumigants, like 1,3-dichIoropropene and metham-sodium (forming methyl isothiocyanate) diffuse into the atmosphere, thus presenting a hazard to people in the surroundings. A method is described in which a large volume (50 PI) of extractant, used to desorb the compounds from charcoal, is injected into a GC, equipped with two capillary columns. By way of Deans switching, the solvent is separated from the compounds of interest. Modification of a GC sampler makes unattended analyses possible.

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Sampling and analysis of the soil fumigants 1,3-dichloropropene and methyl isothiocyanate in the air

Berg

Leistra

Roos³

et al. 1992

Water Air Soil Pollut

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Development and validation of an air monitoring method for 1,3-dichloropropene, trans-1,2,3-trichloropropene, cis-1,2,3-trichloropropene, 1,1,2,3-tetrachloropropene, 2,3,3-trichloro-2-propen-1-ol, and 1,1,2,2,3-pentachloropropane

Cited by 9 publications

References 18 publications

Adsorption/Thermal Desorption with Tenax‐GC for the Collection and Analysis of Polycyclic Aromatic Hydrocarbons and Chlorinated Compounds

Adsorption/Thermal Desorption with Tenax‐GC for the Collection and Analysis of Polycyclic Aromatic Hydrocarbons and Chlorinated Compounds

Determination of soil fumigants in air using tandem capillary gas chromatography after charcoal trapping

Sampling and analysis of the soil fumigants 1,3-dichloropropene and methyl isothiocyanate in the air

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