Direct immersion single drop micro-extraction method for multi-class pesticides analysis in mango using GC–MS

Pano-Farias, Norma S.; Ceballos‐Magaña, Silvia G.; Muñiz‐Valencia, Roberto; Jurado, José Marcos; Alcázar, Ángela; Aguayo‐Villarreal, Ismael Alejandro

doi:10.1016/j.foodchem.2017.05.030

Cited by 64 publications

(23 citation statements)

References 28 publications

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“…Food samples SDME extraction of the organic compounds from food samples is an important application field of SDME technique, it earns nowadays great interest proved by the published papers in recent years. Overview of papers reporting the analysis of various samples, such as tea (Liu et al 2012;Wu et al 2015), wine (Garbi et al 2010Perreira Dos Anjos et al 2015), vegetables (Amrvrazi andTsiropoulos 2009;Kin et al 2009;Wu et al 2016) and fruits (Perreira Dos Anjos et al 2014;Pano-Farias et al 2017) are summarized in the Table 3. All of them were targeted on the determination of the pesticides.…”

Section: Environmental Samplesmentioning

confidence: 99%

“…No special pre-treatment was reported for liquid samples such as wine or coconut water, mainly conventional sonication, acidification, pH adjustment and centrifugation were used (Garbi et al 2010;Perreira Dos Anjos et al 2014;Perreira Dos Anjos et al 2015). On the other hand, more difficult pre-treatment was required for solid samples prior to the extraction step (Amrvrazi and Tsiropoulos 2009;Kin et al 2009;Liu et al 2012;Wu et al 2015;Wu et al 2016;Pano-Farias et al 2017). DI was the most occurred mode of SDME (Amrvrazi and Tsiropoulos 2009;Garbi et al 2010;Perreira Dos Anjos et al 2014;Perreira Dos Anjos et al 2015;Pano-Farias et al 2017).…”

Section: Environmental Samplesmentioning

confidence: 99%

“…On the other hand, more difficult pre-treatment was required for solid samples prior to the extraction step (Amrvrazi and Tsiropoulos 2009;Kin et al 2009;Liu et al 2012;Wu et al 2015;Wu et al 2016;Pano-Farias et al 2017). DI was the most occurred mode of SDME (Amrvrazi and Tsiropoulos 2009;Garbi et al 2010;Perreira Dos Anjos et al 2014;Perreira Dos Anjos et al 2015;Pano-Farias et al 2017). For the extraction of 8 pesticides from cucumber and strawberries, the HS mode was selected and its application was compared to headspace solid phase microextraction (HS-SPME) and solid phase extraction (SPE) (Kin et al 2009).…”

Section: Environmental Samplesmentioning

confidence: 99%

See 2 more Smart Citations

Present state and applications of single drop microextraction for the determination of harmful organic compounds and pollutants

Zichová¹,

Brisudová²,

Hrouzková³

2018

Nova Biotechnologica Et Chimica

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Single drop microextraction (SDME) nowadays earns an increasing attention by scientists due to its simplicity, low cost and the need for only common laboratory equipment. This microextraction technique combines sample cleanup and pre-concentration of analytes in one step. Furthermore, a significant reduction in the amount of organic solvents needed comparing to standard LLE techniques places SDME into the position of environmental friendly extraction techniques. SDME is a straightforward technique in which a micro-drop of solvent is suspended from the tip of a conventional micro-syringe and then it is in a direct contact with a sample solution in which it is immiscible or it could be suspended in the headspace above the sample. The paper overviews developments of the state-of-the-art SDME techniques for the extraction of harmful organic compound and pollutants from environmental, food and biological matrices. Key extraction parameters essential for SDME performance were described and discussed.

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Section: Environmental Samplesmentioning

confidence: 99%

Section: Environmental Samplesmentioning

confidence: 99%

Section: Environmental Samplesmentioning

confidence: 99%

See 1 more Smart Citation

Present state and applications of single drop microextraction for the determination of harmful organic compounds and pollutants

Zichová¹,

Brisudová²,

Hrouzková³

2018

Nova Biotechnologica Et Chimica

View full text Add to dashboard Cite

show abstract

“…The chromatogram for spiked sample matrix with known concentrations of pesticides is shown in Figure 2. The proposed method has also been compared to the reported methods [32][33][34][35][36] for pesticides as shown in Supporting Information Table S4.…”

Section: Real Sample Analysismentioning

confidence: 99%

Dispersion‐assisted quick and simultaneous extraction of 30 pesticides from alcoholic and non‐alcoholic drinks with the aid of experimental design

Jha

Singh

Kumari

et al. 2018

J of Separation Science

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The presence of pesticides in food items and beverages is a big threat to humankind, and their quantitative estimation with high precision and accuracy is always a challenge for analytical chemists. Hence, a simple and rapid method is proposed for the simultaneous determination of 30 pesticides in beverages (alcoholic and non-alcoholic drinks). The proposed method hyphenated with triple quadrupole liquid chromatography mass spectrometry has only 2 min chromatographic runtime for the analysis of all the pesticides. All the factors affecting the extraction yield have been optimized using an experimental design; and under optimized conditions, the developed method has been validated. The detection limits for all the pesticides were in the range of 0.001-0.348 μg/L with good linearity in the concentration range of 0.01-80.0 μg/L. The coefficient of determination was in the range of (R ) ≥ 0.977 to 0.999 for all the pesticides. The method was also checked for the precision of the relative standard deviation, which was below 4.75 (intra-day) and 8.96% (inter-day). The recovery of the method was 92-138%.

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“…Gas chromatography, coupled to different detectors, is used for the analysis of volatile and semi-volatile pesticides. However, the mass spectrometer detector is the most widely used due to its high selectivity and sensitivity and capability to detect compounds with different chemicals [17][18][19].…”

Section: Introductionmentioning

confidence: 99%

Determination of Diazinon and Carbofuran Residue Levels in Apples Kept in Cold Storage Depots in Karaman Province, Turkey

Kiliçel¹,

Karapınar²,

Serin³

2018

Asian J. Chem.

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In this study, two pesticides viz., diazinon and carbofuran residue levels that is used in agricultural spraying in apple samples that were harvested in 2014 harvest season and kept in cold storage in Karaman province, were examined by gas chromatography-mass spectrometer (GC-MS) and gas chromatography-flame-ionisation detector (GC-FID) method. The samples that were taken from 6 different cold storages in the region at 5 different time zones, were kept in laboratory in refrigerator at + 4 °C. The residue levels of diazinon and carbofuran pesticides in apple samples were determined. In order to identify pesticides residues at least three apple samples that were chosen randomly, were homogenized by homogenizator. In extract of samples QuEChERS method was used since it is fast, easy, lowcost, effective and reliable method. The residues of pesticides were taken from this homogenate with acetonitrile and given to GC-MS equipment in a suitable way. According to the results, carbofuran and diazinon pesticides types that are forbidden in Turkey, were determined in large amount of samples.

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Direct immersion single drop micro-extraction method for multi-class pesticides analysis in mango using GC–MS

Cited by 64 publications

References 28 publications

Present state and applications of single drop microextraction for the determination of harmful organic compounds and pollutants

Present state and applications of single drop microextraction for the determination of harmful organic compounds and pollutants

Dispersion‐assisted quick and simultaneous extraction of 30 pesticides from alcoholic and non‐alcoholic drinks with the aid of experimental design

Determination of Diazinon and Carbofuran Residue Levels in Apples Kept in Cold Storage Depots in Karaman Province, Turkey

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