The electrical activation characteristics of Si+ and Be+ ions implanted into InGaAsP (λ=1.3 μm) grown lattice matched to InP by metalorganic molecular beam epitaxy were studied as a function of ion dose (5×1012–5×1014 cm−2), annealing time (3–60 s) and annealing temperature (575–750 °C). Maximum doping concentrations of ∼2×1019 cm−3 were obtained for both Si+ and Be+, with activation energies for electrical activation of 0.58 and 0.39 eV, respectively. Multiple energy F+ or H+ implants can be used to produce high resistance layers for isolation purposes—maximum sheet resistances of ∼8×106 Ω/⧠ or ∼106 Ω/⧠ for initially p+ or n+ InGaAsP, respectively, were obtained for F+ implants followed by annealing near 450 °C. Smooth, anisotropic dry etching of the InGaAsP is obtained with electron cyclotron resonance CH4/H2/Ar discharges at low dc biases. The etch rates are the same for both n+ and p+ quaternary layers and are independent of the doping level.