Abstract. Since melt-textured rare earth (RE)-system superconducting bulk can trap high magnetic field, it acts as a quasi-permanent magnet stronger than conventional permanent magnets. Large-sized single-domain DyBa 2 Cu 3 O x (Dy-123) system bulks about 48 mm in diameter and 15 mm in thickness were prepared with a seeding and temperature gradient method in air. Dy-123 and Dy 2 BaCuO 5 (Dy-211) powders were mixed in molar ratios of 1:0.3. The pellets were partially melted at 1,070 o C. When the top temperature of the sample reached 980 o C, Nd-123 seed crystal was placed on the top surface of the bulk. Then, the samples were cooled from 980 o C to 930 o C, and then with furnace cooling. Finally, the samples were annealed in pure oxygen atmosphere. When magnetic field of 1.5 T was applied to the samples, the maximum trapped magnetic field of 0.7 T was trapped at 77.3 K in the samples prepared with the cooling time for 600 hr and 700 hr from 980 o C to 930 o C. Only 0.2 T was trapped in the sample prepared with the cooling time for 1,000 hr, whose bottom part was decomposed due to long time heating.
IntroductionThe melt-textured DyBa 2 Cu 3 O x (Dy-123) system superconductors which were grown by means of a top seeding and temperature gradient method have high potential for superconductivity applications, since they exhibit higher critical current density (J c ) in high magnetic field compared to melt-textured YBCO superconductors [1][2][3][4]. It was reported that high magnetic field of 1.9 T was trapped at 77.3 K in the presence of 7 T applied parallel to the c-axis for Dy-123 bulk superconductor [5], A large-sized single-domain Dy-123 Superconductor, therefore, is expected for large-scale applications, flywheels, magnetic bearings, magnetic separation, etc.In the previous papers [6][7][8], superconducting properties of melt-textured bulk of Dy-123 system with different molar Dy-123/Dy-211 ratios was studied. Here, both J c and trapped magnetic field increased with the amount of Dy-211. And single-domain bulks, 48 mm in diameter and 15 mm in thickness, were prepared in air. When magnetic field of 1.5 T was applied to the sample, 0.7 T was trapped at 77.3 K. In this report, we investigated the effect of the cooling rate from 980 o C to 930 o C on