Volatile organic compounds (VOCs) emitted from smoldering mosquito coils containing various atomic hydrogen/carbon (H/C) ratios in different relative humidity were examined. The concentrations of individual VOCs were determined using a preconcentrator-gas chromatography/mass spectrometer (GC/MS) and a flame ion detector (FID). Up to 72 VOCs were found. It is noteworthy that benzene and 1,3-butadiene, human carcinogenic substances, were emitted by all tested mosquito coils during burning. The five types of mosquito coils studied had atomic H/C ratios ranging from 1.23 to 1.57, yielding total VOC emission rates and factors of 7,295.72-14,308.17 µg hr -1 and 3,192.78-6,835.03 µg g -1 , respectively. VOC emissions were significantly influenced by the carbon, hydrogen and oxygen contents of coils. According to the analyses of VOC emissions, mosquito coils containing the lowest H/C ratio, a low oxygen content, with suitable additives such as CaCO 3 are recommended for minimizing total VOC emission.