Mild steel has applications in construction, automobiles, mechanical engineering and general purpose fabrication, fencing, cages, frames, furniture components for different shapes, pipelines and other in industries. Cu-Fe-Ni alloy coating with different concentration of Ni was produced on low carbon steel substrate by electrodeposition in this research. This technique is favorable to us because of its low cost and easy to approach. The electrolytic bath contained the 31.92g/l CuSO4, 54.2 g/l FeSO4, NiSO4.7H2O (0.00 g/l, 14.04 g/l, 28.08 g/l, 42.12 g/l) and 15.4 g/l H3BO3 as buffer to maintain pH at 3. The electrodeposition is done at suitable deposition parameters. The effect of Ni concentration on the surface morphology, structure and mechanical properties of coating were revealed by scanning electron microscope (SEM), X-ray diffraction (XRD) analysis and Vicker hardness tester respectively. Obtained results showed that with the increase in Ni content grain size increases and elongation decreases while the mechanical properties increases. The thickness of deposited Cu-Fe-Ni alloys has decreasing trend of thickness with increasing of Ni contents.