2019
DOI: 10.1088/1742-6596/1386/1/012016
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Effect of exfoliation method on graphite oxide. A comparison between exfoliation by ball milling and sonication in different media

Abstract: Graphene oxide and reduced graphene have been exfoliated from graphite oxide synthesized by Hummer’s method. In order to establish a comparison, the exfoliation process was performed using two different methods, high energy ball milling and sonication. Each one was studied in two different media, organic solvent N-methyl 2 pyrrolidone and deionized water, obtaining four different products. The quality of the graphene and graphene oxides was studied using Raman spectroscopy. Structural characterization was perf… Show more

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Cited by 3 publications
(2 citation statements)
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“…Figure 4b exhibits the Raman spectra of the pristine-CNW and CNW/ITO micro-structure. To the best of our knowledge, D (1350 cm −1 ), G (1580 cm −1 ), and 2D (2700 cm −1 ) are the common band of carbon materials, and a high D band and D band (shoulder band) is a unique band that can only be found in defected graphite [18][19][20]. In the Raman spectra of the CNW/ITO micro-structure from Figure 4b, it shows a low I D /I G ratio (1.71) with a low D band than pristine-CNW.…”
Section: Resultsmentioning
confidence: 97%
“…Figure 4b exhibits the Raman spectra of the pristine-CNW and CNW/ITO micro-structure. To the best of our knowledge, D (1350 cm −1 ), G (1580 cm −1 ), and 2D (2700 cm −1 ) are the common band of carbon materials, and a high D band and D band (shoulder band) is a unique band that can only be found in defected graphite [18][19][20]. In the Raman spectra of the CNW/ITO micro-structure from Figure 4b, it shows a low I D /I G ratio (1.71) with a low D band than pristine-CNW.…”
Section: Resultsmentioning
confidence: 97%
“…Ball milling has also been investigated to exfoliate graphite oxide. Nevertheless, the quality and the degree of oxidation are highly affected by the solvent, with mainly reduced graphene oxide achieved when using water [52].…”
Section: Graphene Oxidementioning
confidence: 99%