Effect of mechanochemical surface preparation on bonding to zirconia of a tri-&lt;i&gt;n&lt;/i&gt;-butylborane initiated resin

Akazawa, Nobutaka; Koizumi, Hiroyasu; Nogawa, Hiroshi; Nakayama, Daisuke; Kodaira, Akihisa; Matsumura, Hideo

doi:10.4012/dmj.2016-099

Cited by 9 publications

(17 citation statements)

References 20 publications

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“…Previous studies have reported that air-abrasion of silica-coated alumina particles (Rocatec system) can chemically modify material surfaces, leading to improve bonding properties [37][38][39][40] . Alumina air-abrasion has been considered to have a mechanical effect on adhesive bonding, but the chemical effects have not been clarified so far.…”

Section: Discussionmentioning

confidence: 99%

Chemical alteration of Ag-Pd-Cu-Au alloy surface by alumina air-abrasion and its effect on bonding to resin cement

et al. 2019

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The goal of this study was to investigate the chemical alteration of a dental alloy surface by alumina air-abrasion and its effect on bonding to resin cement. Alumina air-abrasion was carried out on an Ag-Pd-Cu-Au alloy. The surface morphology and chemical state of the abraded alloy were characterized. The effect of the air-abrasion on the shear bond strength between the alloy and a methyl methacrylate/tri-n-butyl borane (MMA/TBB) resin cement with some primers was evaluated. The surface characterization revealed that the alumina air-abrasion mechanically roughened and chemically altered the surface. The chemical alterations had two effects:(1) abraded alumina particles remained on the alloy surface and (2) copper ions were oxidized in the alloy surface. As the result, the shear bond strength test indicated that 10-methacryloyloxydecyl dihydrogen phosphate (MDP) contained primer worked with the abraded alloy surface, whereas it did not work with the non-abraded alloy surface.

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Section: Discussionmentioning

confidence: 99%

Chemical alteration of Ag-Pd-Cu-Au alloy surface by alumina air-abrasion and its effect on bonding to resin cement

et al. 2019

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“…Although many dental techniques [32] have been extensively investigated to improve the bond strength of resin to zirconia ceramics, there is no established protocol that can produce a stable bond which can be easily used at the present time. To achieve higher retention, prevent micro-leakage, and increase the fracture and fatigue resistance of restorations, many studies are under way [13, 26, 27]. However, the subpressure infiltration technique has not been applied in the dental adhesion.…”

Section: Discussionmentioning

confidence: 99%

“…Usually, the strength of low-viscosity adhesives is lower than that of high-viscosity adhesives [39, 40]. Additionally, primers or luting agents containing functional monomers could increase the chemical bonding and wettability [26,41]. The configuration of the zirconia surface could affect the infiltration as well, and the subpressure value and action time could also affect the infiltration capacity.…”

Section: Discussionmentioning

confidence: 99%

“…Previous research has suggested that sandblasting before sintering is a useful method for significantly increasing the surface roughness, and it is considered to reverse the transformation (m→t) caused by sandblasting during the sintering process [19,25]. Additionally, Nobutaka et al [26] focused on the effect of a primer on bonding to the zirconia. Wei et al [27] suggested that a high pressure blowing method could improve the adhesion of resin to dentin.…”

Section: Introductionmentioning

confidence: 99%

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The effect of subpressure on the bond strength of resin to zirconia ceramic

Zhuge

Zhang

et al. 2017

PLoS ONE

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ObjectiveThis study was conducted to investigate the effect of subpressure on the bond strength of resin to zirconia ceramic. The subpressure would create a pressure gradient which could clean out the bubbles in the adhesives or bonding interface.MethodsTwenty-eight pre-sintered zirconia discs were fabricated. Half of them were polished (group P, n = 14), and the rest were sandblasted (group S, n = 14). After sintered,the surface roughness of the zirconia discs was measured. Then, they were randomly divided into two subgroups (n = 7). The groups were named as follows: PC: P + no additional treatments; PP: P + 0.04 MPa after application of adhesives; SC: S + no additional treatments; and SP: S + 0.04 MPa after application of adhesives. Resin columns were bonded to the zirconia specimens to determine shear bond strength (SBS). The bonding interfaces were observed and the fracture modes were evaluated. Statistical analysis was performed on all data.ResultsThe surface roughness of group S was significantly higher than that of group P (P<0.05). The SBS values were PC = 13.48 ± 0.7 MPa, PP = 15.22 ± 0.8 MPa, SC = 17.23 ± 0.7 MPa and SP = 21.68 ± 1.4 MPa. There were significant differences among the groups (P<0.05). Scanning electron microscopy (SEM) results showed that the adhesives of group SP and PP were closer and denser to the zirconia ceramic than that of group PC and SC. The proportion of the mixed fracture mode significantly increased after adding subpressure (P< 0.05).ConclusionSubpressure can improve the shear bond strength of resin to zirconia ceramics and increase micro-infiltration between the adhesives and the zirconia ceramics, especially on the rough surfaces.

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“…The successful primer is a solution of MDP and VBATDT dispersed in acetone and the ratio between the two monomers is not disclosed by the manufacturer. Considering that this primer was developed for bonding to metal infrastructures [26], it can be hypothesized that the formulation is not optimized for Y-TZP-based substrates, and that variations in the ratio between the two monomers may clarify the importance of each of them on bonding to Y-TZP.…”

Section: Introductionmentioning

confidence: 99%

The Role of a MDP/VBATDT-Primer Composition on Resin Bonding to Zirconia

Aggarwal

Souza

2018

Metals

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Yttria-tetragonal zirconia polycrystal (Y-TZP) is a difficult substrate to bond to due to the absence of a glass phase and the material's chemical inertness. This study evaluated the effect of two monomers for metal, MDP (10-methacryloyloxydecyl dihydrogen phosphate) and VBATDT (6-(4-vinylbenzyl-n-propyl)amino-1,3,5-trizaine-2,4-dithiol) on bond strength to Y-TZP. Seven combinations with different concentrations of MDP and VBATDT-monomers (0.0, 0.1, 0.5, or 1.0 wt %) in acetone solution were developed and applied to the surface of Y-TZP slabs, which were bonded to composite resin substrates using a resin cement under standard loading. Non-primed samples were used as controls. Bonded specimens were cut for microtensile testing and tested after either 48 h or 180 days in water storage at room temperature. All samples from control group (no primer) and MV5 group (0% MDP/0.5% VBATDT) debonded spontaneously. Two-way ANOVA showed that the primer had a significant effect (p < 0.001) on bond strength to zirconia, whilst storage time did not (p = 0.203). Tukey HSD (honest significant difference) test indicated that groups with at least 0.5% of each monomer resulted in higher initial bond strength values. Although chemical bonding to zirconia is credited to MDP, a correct balance between MDP and VBATDT may imply in better bond strength results. The minimum concentration of each monomer should not be lower than 0.5 wt %.

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Effect of mechanochemical surface preparation on bonding to zirconia of a tri-<i>n</i>-butylborane initiated resin

Cited by 9 publications

References 20 publications

Chemical alteration of Ag-Pd-Cu-Au alloy surface by alumina air-abrasion and its effect on bonding to resin cement

Chemical alteration of Ag-Pd-Cu-Au alloy surface by alumina air-abrasion and its effect on bonding to resin cement

The effect of subpressure on the bond strength of resin to zirconia ceramic

The Role of a MDP/VBATDT-Primer Composition on Resin Bonding to Zirconia

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