Effect of the Fractional Distillation on an Increment Patchouli Alcohol Content in Patchouli Oil

Aisyah, Yuliani; Anwar, Sri Haryani; Annisa, Yulia

doi:10.5220/0009957100800085

Cited by 3 publications

(3 citation statements)

References 0 publications

Supporting

Mentioning

Contrasting

Order By: Relevance

“…Most significantly, patchouli oil acts as a fixative agent. A fixative agent is a substance that is used to reduce the rate of evaporation and can increase the stability of the mixture when added to more volatile components [7]. Its fixative properties give perfumes a strong and lasting character when combined with other essential oils [8].…”

Section: Introductionmentioning

confidence: 99%

Characterization of Bioactive Compounds from Patchouli Extracted via Supercritical Carbon Dioxide (SC-CO2) Extraction

et al. 2022

View full text Add to dashboard Cite

Patchouli extracts and oils extracted from Pogostemon cablin are essential raw material for the perfume and cosmetics industries, in addition to being used as a natural additive for food flavoring. Steam distillation is a standard method used for plant extraction. However, this method causes thermal degradation of some essential components of the oil. In this study, patchouli was extracted with supercritical carbon dioxide (SC-CO2) under different conditions of pressure (10–30 MPa) and temperature (40–80 °C). The chemical components of the crude extracted oil and the functional group were characterized using gas chromatography-mass spectrometry (GC-MS) and Fourier Transform Infrared Spectroscopy (FT-IR). The extraction with supercritical carbon dioxide was shown to provide a higher yield (12.41%) at a pressure of 20 MPa and a temperature of 80 °C. Patchouli alcohol, Azulene, δ-Guaiene, and Seychellene are the main bioactive compounds that GC-MS results have identified. FTIR spectra showed alcohol, aldehyde, and aromatic ring bond stretching peaks. Extraction of patchouli with supercritical carbon dioxide provided a higher yield and a better quality of the crude patchouli oil.

show abstract

Section: Introductionmentioning

confidence: 99%

Characterization of Bioactive Compounds from Patchouli Extracted via Supercritical Carbon Dioxide (SC-CO2) Extraction

et al. 2022

View full text Add to dashboard Cite

show abstract

“…Currently, Indonesia can produce nine types of essential oils, namely: clove oil, ylang oil, patchouli oil, fragrant root oil, nutmeg oil, eucalyptus oil, cinnamon oil and citronella oil. There are six types of essential oils that are most prominent in Indonesia,namely: nutmeg oil, patchouli oil, eucalyptus oil, ylang ylang oil, clove oil and citronella oil [1]. Increasing production of citronella essensial oil this can be seen from the many modern products that have been circulating, such as cosmetics and aromatherapy, which are produced from this oil.…”

Section: Introductionmentioning

confidence: 99%

Physicochemical Analysis Using Gas Chromatogrphy Mass Spectrophotometer (GCMS) on the Quality of Citronella Oil (Cymbopogon nardus L.)

Itawani,

Hayati,

Munawar

2024

IOP Conf. Ser.: Earth Environ. Sci.

View full text Add to dashboard Cite

Indonesia is known as a country that has biological forests which can be used as a source of essential oils. The levels of chemical compounds that make up citronella oil are not fixed and depend on several factors such as distillation. Distillation using traditional methods is a production process that has been identical for generations used by farmers, usually this distillation uses wood fuel and takes 5 hours. Meanwhile, distillation with electrical energy only takes 4-5 hours. This research was conducted at the Laboratory of Chemical Analysis, Faculty of Mathematics and Natural Sciences, Syiah Kuala University, Banda Aceh. This research was conducted from January 2023 to June 2023. The results showed that distillation using the traditional method had 15 chemical compounds and consisted of 3 active ingredients, namely citronellal (42.48%), geraniol (17.60%) and citronellol ( 13.67%) while the results of the distillation by the electric method have 21 compounds and also consist of 3 active ingredient components, namely citronellal (40.87%), geraniol (16.53%) and citronellol (17.68%).

show abstract

“…Other fractional distillation process specifications include the feed flow rate, composition, thermal properties of the feed, the desired distillate composition, and the expected yield [25]. Some important factors that affect fractional distillation are reflux ratio, pressure, temperature, column-tray configuration, and fractional column length [16,25,26].…”

Section: Introductionmentioning

confidence: 99%

Optimization of the Vacuum Fractional Distillation Process for Enhancing the α-Guaiene of Patchouli Oil with Response Surface Methodology

Widyasanti,

Nurjanah,

Nurhadi

et al. 2023

Separations

View full text Add to dashboard Cite

α-guaiene is one of the primary sesquiterpene compounds used as a flavor and fragrance agent in patchouli oil. The fraction of patchouli oil that is rich in α-guaiene has been successfully isolated. In the present work, α-guaiene was isolated from crude patchouli oil through vacuum fractional distillation followed by GC-MS identification. Three important process parameters—feed volume, reflux ratio, and applied run pressure—were investigated and optimized using Box–Behnken design. The research methodology was an experimental laboratory using response surface methodology (RSM) with a feed volume level from 75 mL to 125 mL, a reflux ratio from 10:1 to 30:1, and an applied run pressure from 5 mmHg to 15 mmHg. The α-guaiene-enriched fraction was found in the first distillate fraction patchouli. The optimum condition that generated α-guaiene fraction at 44.70% purity was the treatment with a feed volume of 75 mL, a reflux ratio of 24:1, and applied run pressure of 14.80 mmHg. Results indicated that feed volume did not significantly affect the α-guaiene content, while the applied run pressure and reflux ratio used had a significant effect. A quadratic mathematical model with R2 0.861 and validation 96.14% was suitable for predicting the optimum α-guaiene fraction content during the vacuum fractional distillation process.

show abstract

Effect of the Fractional Distillation on an Increment Patchouli Alcohol Content in Patchouli Oil

Cited by 3 publications

References 0 publications

Characterization of Bioactive Compounds from Patchouli Extracted via Supercritical Carbon Dioxide (SC-CO2) Extraction

Characterization of Bioactive Compounds from Patchouli Extracted via Supercritical Carbon Dioxide (SC-CO2) Extraction

Physicochemical Analysis Using Gas Chromatogrphy Mass Spectrophotometer (GCMS) on the Quality of Citronella Oil (Cymbopogon nardus L.)

Optimization of the Vacuum Fractional Distillation Process for Enhancing the α-Guaiene of Patchouli Oil with Response Surface Methodology

Contact Info

Product

Resources

About