“…Prior to weighing and mixing, the oxides and carbonate powder were pre-annealed at 110°C for more than 24 h in air to release moisture. Then, the powders were weighed in a glove box, homogenized in an agate mortar for one hour, and put placed into alumina crucibles and calcined at 930°C for 40 hours in air 24,[27][28][29][30][31] . The obtained precursors were again homogenized, pressed into pellets (with the a diameter of 16 mm), sintered in a horizontal tube furnace in flowing oxygen (10 ml/min) at about approximately 1060°C for 72 h, then cooled to 520°C and, held at this temperature for 24 h, subsequently cooled in the furnace to room temperature 31 .…”