Elaboration of the technique of atomic emission detection with inductively coupled plasma of platinum metals in chamotte waste with autoclave sample preparation and design of the experiments

Decomposition of samples of used ceramic-based automotive catalytic converters in analytical autoclaves with resistive heating

“…The process of decomposition of samples in autoclaves runs more effectively, while the sample preparation time is reduced, reagent consumption decreases (making it possible to reduce the blank experiment correction), working conditions are improved, and power consump tion and complexity of the sample preparation stage are reduced [12][13][14]. Furthermore, when using analytical autoclaves, it is possible to increase the sample shot as compared with both the fusion method and various ver sions of acid decomposition in open systems without deterioration in the above mentioned parameters char acterizing the efficiency of CSP, which is an important factor for heterogeneous materials, such as ACCs.…”