2012
DOI: 10.1007/s10008-012-1804-6
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Electrodeposition of ZnO coatings from aqueous Zn(NO3)2 baths: effect of Zn concentration, deposition temperature, and time on orientation

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Cited by 16 publications
(8 citation statements)
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“…Additionally, ZnO can be electrodeposited with different out-of-plane orientations, by merely varying some of the deposition conditions [23]. A cohort of differently oriented ZnO coatings were fabricated (figure 1) by selecting the appropriate electrodeposition conditions reported earlier [18] and cycled in hermetically sealed Swagelok cells. These experiments were initiated to examine if the polar 001 crystal face of ZnO had a higher charge storage capacity compared to the non-polar faces.…”
Section: Resultsmentioning
confidence: 99%
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“…Additionally, ZnO can be electrodeposited with different out-of-plane orientations, by merely varying some of the deposition conditions [23]. A cohort of differently oriented ZnO coatings were fabricated (figure 1) by selecting the appropriate electrodeposition conditions reported earlier [18] and cycled in hermetically sealed Swagelok cells. These experiments were initiated to examine if the polar 001 crystal face of ZnO had a higher charge storage capacity compared to the non-polar faces.…”
Section: Resultsmentioning
confidence: 99%
“…In the specific case of ZnO, the morphology of crystallites in differently oriented coatings is the same. The different out of plane orientations arise merely due to the tilting of the hexagonal columns with respect to the substrate normal [18]. As a result, differently oriented coatings do not expose any new crystal faces with high surface energies other than the 001 face.…”
Section: Resultsmentioning
confidence: 99%
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“…S4. It could 19 be seen that some horizontally aligned nanorods appeared with 0.01 M Zn(NO 3 ) 2 ·6H 2 O electrolyte due to the fast preferentially growth along the (0001) direction [21]. Once the concentration of Zn(NO 3 ) 2 ·6H 2 O electrolyte increased to 0.05 M, the surface of electrode was coated by uniform nanospheres due to the isotropic growth from center nuclei [7].…”
Section: 1 V) Andmentioning
confidence: 98%
“…Among these methods, electrodeposition [15,16] of ZnO is a more efficient method to obtain nanostructured ZnO with various morphologies due to its cheap experimental setups, rapid and cost-effective method, low-temperature processing, and precise control of film thickness. This method not only offers a wide range of morphological design options of the nanostructures [17][18][19] but also can realize controlled preparation via easily changing the electrochemical parameters, such as electrodeposition time and potential [20][21][22]. For example, ZnO nanotube arrays (ZNTAs) were successfully synthesized on FTO substrate using one-step electrodeposition method.…”
Section: Introductionmentioning
confidence: 99%