In this study, we fabricated thin-film resistors using CuMn and yttrium targets by DC/RF magnetron cosputtering. CuMnYresistive thin films were deposited onto glass and Al 2 O 3 substrates. e electrical properties and microstructures of CuMn alloy films with different yttrium content were investigated. e CuMnY films were annealed at temperature ranging from 250°C to 350°C in N 2 atmosphere. e phase variation, microstructure, film thickness, and constitutional analysis of CuMnY films were characterized using X-ray diffraction, field emission scanning, and high-resolution transmission electron microscopy and related energy dispersive X-ray analyses (XRD, FESEM, and HRTEM/EDX). It was found that CuMnY alloy films separated into two parts after annealing. e first part is the MnO phase on the bottom side of the film. e second part is an amorphous structure on the upper side of the film. e MnO phase is a microcrystalline that exists in CuMn films, which is dependent on the Y content and annealing temperature. CuMn alloy films with 15.7% yttrium addition annealed at 300°C exhibited higher resistivity ∼4000 μΩ-cm with − 41 ppm/°C of temperature coefficient of resistance (TCR).