1992
DOI: 10.1021/jo00052a036
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Electroorganic chemistry. 140. Electroreductively promoted intra- and intermolecular couplings of ketones with nitriles.

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Cited by 95 publications
(67 citation statements)
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“…Rosaprostol 7 obtained as above was a 1:1 mixture of trans-trans and trans-cis stereoisomers. The overall yield of our synthesis was 42% and was much higher than those reported in the literature (< 20%) [20].…”
Section: Synthesis Of Racemic Rosaprostolcontrasting
confidence: 51%
“…Rosaprostol 7 obtained as above was a 1:1 mixture of trans-trans and trans-cis stereoisomers. The overall yield of our synthesis was 42% and was much higher than those reported in the literature (< 20%) [20].…”
Section: Synthesis Of Racemic Rosaprostolcontrasting
confidence: 51%
“…phase was concentrated and bulb‐to‐bulb distilled to afford pure 1a in 75% yield . For analyses, see . Alternatively, a soln.…”
Section: Methodsmentioning
confidence: 99%
“…• O acoplamento intramolecular de cetonas com O-metiloximas (esquema 4i) 37 em eletrólises a corrente controlada e com nitrilas (esquema 4j) 38 , em potencial constante, também ocorreu com apreciável estereosseletividade. A trans-seletividade (esquema 4i) explica-se pela repulsão eletrônica forte entre as cargas negativas no O e N, no intermediário (J).…”
Section: Esquema 1 Diferentes Produtos Via Diferentes Mecanismos Em unclassified