Charged-particle correlations were measured for the reactions N+ Au and N+ Al at E/A = 75 MeV and for Xe+ Al and Xe+ Sn at E/A = 31 MeV. Relative populations of widely separated states in He, Li, and Be, only weakly a8'ected by side feeding, indicate emission temperatures of T=4 -5 MeV for the ¹induced reactions and values about 1 MeV lower for the Xe-induced reactions. PACS number(s): 25.70.Mn, 25.70.Gh I. INTR. ODUCTION Highly excited nuclear matter can be formed in intermediate-energy heavy-ion reactions. To address questions concerning the statistical properties of hot nuclei, it is important to determine their temperature. Experimental investigations have found evidence for a saturation in emission temperatures for fragments of T=4-6 MeV [1 -27] and evidence for a possible limitation on excitation energy of targetlike residues [28 -42]. However, it is not clear if this saturation of excitation energy arises from an instability of bulk nuclear matter which may be related to a phase transition or from dynamical limitations which may govern the energy dissipation into internal degrees of freedom. Both statistical [43,44] and dynamical [45,46] models predict that nuclear matter at suKciently high temperatures expands due to the action of thermal pressure. The rate of this expansion and the *Present address: