This study aims to determine the temporal distribution and composition of suspended particulate matter in different sizes PM 2.5-10 (Coarse Particle, CP) and PM 2.5 (Fine Particle, FP) for source apportionment analysis. CP and FP samples were collected using the Gent PM 10 stacked filter unit (SFU) sampler at an urban coastal city of Kuala Terengganu, in , Al, Ca, K and Na were mainly in fine particle size range and accounted for ca. 28% of the fine particle mass. The data sets were then analyzed using Principle Component Analysis (PCA) to identify the possible sources of these fine and coarse particles based on their chemical species. For both fractions, the sources were soil dust, marine aerosol, vehicle exhaust, secondary aerosol, road dust and biomass burning. In addition, crustal enrichment factors (cEF) were calculated, and the results were consistent with those of the PCA analysis.