Composite biomass briquette has been synthesized and characterized from a mixture of domestic solid waste and coconut husk using cow dung as a binder. A 170-litre metal drum was used as a kiln for feedstock pyrolysis. The feedstocks were subjected to SEM analysis and proximate analysis. Moreover, an Oxygen Parr Bomb Calorimeter was used to estimate the composite briquette's gross calorific value. Additionally, a LECO 932 CHNS elemental analyzer was utilized to determine the elemental composition of the composite biomass briquette. Subsequently, a Water boiling test was conducted to assess the suitability of the fuel compared to traditional charcoal observing the fuel burning rate, specific fuel consumption, ignition time, and thermal efficiency. The composite biomass briquettes had an optimal high heating value of 19.3 ± 0.1 MJ/kg, ash content of 7.4 ± 0.2%, and 512.03g/ m3 bulk density. The cow dung used as a binder demonstrated excellent lignin composition and adhesive properties. These properties complied with the specifications outlined by the American Society for Testing and Materials (ASTM E791-08) Standard. Based on the findings, further research is recommended to focus on gas emission analysis and comprehensive ultimate analysis of composite biomass briquettes.