Evolution of the zinc compound nanostructures in zinc acetate single-source solution

Wang, Ying; Li, Yinhua; Zhou, Zhengzhi; Zu, Xihong; Deng, Yulin

doi:10.1007/s11051-011-0504-y

Cited by 50 publications

(63 citation statements)

References 54 publications

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“…6 shows that all the samples in the presence of different TGA values have the same characteristic peaks with different absorption amplitudes. The sample without TGA (S1) shows different FTIR absorption pattern which best confirms the formation of zincacetate crystals [43] conforming XRD analysis. The broad absorption band at 3420 cm À 1 can be assigned to the OH group and water.…”

Section: Structural Characterizationsupporting

confidence: 65%

Red luminescence of Zn /ZnO core–shell nanorods in a mixture of LTZA/Zinc acetate matrix: Study of the effects of Nitrogen bubbling, Cobalt doping and thioglycolic acid

Karimipour

Kheshabnia

Molaei

2016

Journal of Luminescence

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Section: Structural Characterizationsupporting

confidence: 65%

Red luminescence of Zn /ZnO core–shell nanorods in a mixture of LTZA/Zinc acetate matrix: Study of the effects of Nitrogen bubbling, Cobalt doping and thioglycolic acid

Karimipour

Kheshabnia

Molaei

2016

Journal of Luminescence

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“…With decreasing initial precursor concentrations, the mechanism produces smaller amounts of particles that have a taller shape. The formation of dumbbells under suitable conditions has also already been observed (Wang et al 2011).…”

Section: Cellulosementioning

confidence: 69%

Microwave solvothermal decoration of the cellulose surface by nanostructured hybrid Ag/ZnO particles: a joint XPS, XRD and SEM study

et al. 2015

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The synthesis of hybrid silver/zinc oxide (Ag/ZnO) decoration on the cellulose surface is described. The structures were characterized with X-ray photoelectron spectroscopy (XPS) and corroborated with X-ray diffraction and scanning electron microscopy. Silver nitrate and zinc acetate dihydrate were used as soluble raw materials. Hexamethylenetetraamine was used as the precipitating and reducing agent. The surface of a-cellulose was always treated by hydrogen peroxide before synthesis with a relatively mild effect manifested in water contact angle measurement and XPS high-resolution spectra. The Ag/ZnO decoration system was identified as a true nanodispersed metal/semiconductor hybrid with a unique collective plasmonic structure observed on Ag 3d core lines for the first time. A series of experiments with a single precursor solution contributed to the characterization of the interaction of Ag ? and Zn 2? species with the surface and to the description of the reaction mechanism in the mixed precursor solution. In contrast to previous reports, a specific interaction between the cellulose substrate and Zn 2? was observed. No specific non-thermal effects of microwave heating were observed.

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“…Some works demonstrate the huge influence that ambient humidity 7 , precursor 8 or solvent 9 have on the pyrolysis of zinc acetate dihydrate (ZAD) and the subsequent formation of ZnO 10,11,12 . Other reports highlight the appearance of different intermediate compounds, such as hydroxyl-or anhydrous acetates 13 , oxo-acetates 14 or hydrated hydroxyl-acetates 15 when similar ZAD species degrade, giving rise to nanowires 16 , nanobelts 17 or other nanostructures 18,19,20 .…”

Section: Introductionmentioning

confidence: 99%

Study of a sol–gel precursor and its evolution towards ZnO

Gómez-Núñez

López

Alonso-Gil

et al. 2015

Materials Chemistry and Physics

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Abstract:The processes involved in the assembly of zinc acetate dihydrate {Zn(CH 3 COO) 2 ·2H 2 O} and ethanolamine (H 2 NCH 2 CH 2 OH), with or without 2-methoxyethanol as solvent, have been analysed by infrared spectra, mass spectrometry, nuclear magnetic resonance, powder X-ray diffraction and computational studies. Thermal evolution of the mixtures was characterized by thermoanalytical and structural techniques (thermogravimetry, differential thermal analysis, differential scanning calorimetry, X-ray diffraction and X-Ray photoelectron spectroscopy). Computational studies together with experiments served to thoroughly describe the precursor and its decomposition. The thermal decomposition of the mixture and its transformation into crystalline ZnO take place in a temperature range between 50 and 450 °C through different processes. With solvent, the processes need temperatures

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Evolution of the zinc compound nanostructures in zinc acetate single-source solution

Cited by 50 publications

References 54 publications

Red luminescence of Zn /ZnO core–shell nanorods in a mixture of LTZA/Zinc acetate matrix: Study of the effects of Nitrogen bubbling, Cobalt doping and thioglycolic acid

Red luminescence of Zn /ZnO core–shell nanorods in a mixture of LTZA/Zinc acetate matrix: Study of the effects of Nitrogen bubbling, Cobalt doping and thioglycolic acid

Microwave solvothermal decoration of the cellulose surface by nanostructured hybrid Ag/ZnO particles: a joint XPS, XRD and SEM study

Study of a sol–gel precursor and its evolution towards ZnO

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