2009
DOI: 10.1063/1.3236365
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Experimental method for in situ determination of material textures at simultaneous high pressure and high temperature by means of radial diffraction in the diamond anvil cell

Abstract: We introduce the design and capabilities of a resistive heated diamond anvil cell that can be used for side diffraction at simultaneous high pressure and high temperature. The device can be used to study lattice-preferred orientations in polycrystalline samples up to temperatures of 1100 K and pressures of 36 GPa. Capabilities of the instrument are demonstrated with preliminary results on the development of textures in the bcc, fcc, and hcp polymorphs of iron during a nonhydrostatic compression experiment at s… Show more

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Cited by 44 publications
(44 citation statements)
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“…At present, works are under way to extend the measurements into several directions: (i) larger P, T, and composition ranges [245,270]; (ii) finer interpretation of the experimental data with polycrystal plasticity models [253]; and (iii) complex deformation history, such as sinusoidal oscillations [283]. These works will allow, in the future, clarifying the combined effects of P and T on MgO and (Mg,Fe)O plasticity.…”
Section: Experimental Identification Of Individual Deformation Mechanmentioning
confidence: 99%
See 1 more Smart Citation
“…At present, works are under way to extend the measurements into several directions: (i) larger P, T, and composition ranges [245,270]; (ii) finer interpretation of the experimental data with polycrystal plasticity models [253]; and (iii) complex deformation history, such as sinusoidal oscillations [283]. These works will allow, in the future, clarifying the combined effects of P and T on MgO and (Mg,Fe)O plasticity.…”
Section: Experimental Identification Of Individual Deformation Mechanmentioning
confidence: 99%
“…A limitation of the DAC is that pressure and deformation cannot be decoupled. Despite these limitations, the DAC is a useful tool for investigating plastic properties up to 300 GPa at ambient temperature [244] with developments under way to allow for performing high-T experiments, either using resistive heating elements [245] or lasers [246]. Stress in DAC experiments is typically assumed to be axial with cylindrical symmetry around the compression direction [247] and with low pressure gradients across the sample.…”
Section: Experimental Devicesmentioning
confidence: 99%
“…The first run was performed at HPCAT beamline 16-ID-B in a modified Mao-Bell DAC with 70° lateral openings for radial diffraction (Liermann et al 2009). The sample was loaded into a boron epoxy gasket inside of a Kapton insert (Merkel and Yagi 2005).…”
Section: Runmentioning
confidence: 99%
“…To this day, the determination of active deformation mechanisms in iron at core conditions remains an active field of research (Poirier and Price, 1999;Wenk et al, 2000b;Merkel et al, 2004;Miyagi et al, 2008;Liermann et al, 2009) and more experiments will be needed to properly constrain those parameters.…”
Section: Plastic Propertiesmentioning
confidence: 99%