GC–MS analysis of bioactive components and synthesis of gold nanoparticle using Chloroxylon swietenia DC leaf extract and its larvicidal activity

Balasubramani, Govindasamy; Ramkumar, Rajendiran; Krishnaveni, Narayanaswamy; Sowmiya, Rajamani; Deepak, Paramasivam; Dhayalan, Arul; Perumal, Pachiappan

doi:10.1016/j.jphotobiol.2015.03.016

Cited by 48 publications

(16 citation statements)

References 31 publications

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“…The elements present in the formed AuNPs were identified by EDX (Table ). Leaf elemental gold produced three clear signals at 2.120, 9.712, and 11.8 keV, whereas seed elemental gold produced a relatively lower single signal at 2.120 keV . The difference in number and intensities of signals for both leaf and seed AuNPs can be ascribed to the assembly and exposure of leaf AuNPs (FE‐SEM images), while the remaining signals could be attributed to biomolecule‐protected AuNPs.…”

Section: Resultsmentioning

confidence: 95%

Green synthesis and bactericidal activities of isotropic and anisotropic spherical gold nanoparticles produced using Peganum harmala L leaf and seed extracts

Moustafa

Alomari

2019

Biotech and App Biochem

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Shape, size, and homogeneity affect the biological activity of gold nanoparticles (AuNPs) in nanomedicine and catalytic applications. Here we biosynthesized monodispersed isotropic and polydispersed anisotropic spherical AuNPs from leaf and seed extract broths of the medicinal plant Peganum harmala L. (Ph. L). Synthesized AuNPs were characterized by ultraviolet-visible spectroscopy, Fourier-transform infrared spectroscopy (FT-IRS), field-emission scanning electron microscopy (FESEM), X-ray diffraction (XRD), energy-dispersive X-ray spectroscopy (EDX), and transmission electron microscopy (TEM). The antimicrobial activity of AuNPs against Gram-negative (Escherichia coli) and Gram-positive (Staphylococcus aureus) human pathogens was also assessed. Leaf-and seed-derived AuNPs had characteristic localized surface plasmon resonances of 530 and 578 nm, respectively. TEM, FE-SEM, EDX, and XRD revealed the formation of elemental face-centered cubic spherical monodispersed isotropic AuNPs of average size 43.44 nm and polydispersed anisotropic AuNPs of average size 52.04 nm from leaf and seed extract broths, respectively. FT-IR revealed polyphenols and alcohols as responsible for AuNP capping, reduction, and protection. Anisotropic AuNPs showed no antibacterial activity, whereas isotropic AuNPs showed good inhibition of both E. coli and S. aureus. This represents a simple and ecofriendly protocol for the green synthesis of monodispersed isotropic spherical AuNPs, which may have value in a variety of applications.

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Section: Resultsmentioning

confidence: 95%

Green synthesis and bactericidal activities of isotropic and anisotropic spherical gold nanoparticles produced using Peganum harmala L leaf and seed extracts

Moustafa

Alomari

2019

Biotech and App Biochem

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“…It is known that the position of the OH‐absorption bands depend on the degree of strength of hydrogen bonding, and shifts to lower wave numbers when hydrogen bonding becomes stronger . Consistent bands at 2939 and 1384 cm −1 may be assigned to the group alkanes with stretching vibration of CH . Bands located at 1326 and 1104 cm −1 were due to CN stretching vibration of aromatic and aliphatic amines, respectively .…”

Section: Resultsmentioning

confidence: 99%

Biosynthesis of gold nanoparticles using green roof species Portulaca grandiflora and their cytotoxic effects against C6 glioma human cancer cells

Thirunavukkarasu

Arockiaraj

Vijayaraghavan

2016

Env Prog and Sustain Energy

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Leaf and stem extracts of popular green roof vegetation, Portulaca grandiflora, were used for the synthesis of gold nanoparticles. The synthesized gold nanoparticles were characterized using UV–visible spectroscopy, Fourier transform infrared (FTIR) spectroscopy, X‐ray diffraction (XRD), scanning electron microscopy (SEM) and transmission electron microscopy (TEM) analysis. FTIR results indicated the presence of proteins and polyphenols in plant extracts which were responsible for the reduction and stabilization of gold nanoparticles. SEM and TEM images confirmed the formation of spherical, rhombus, triangular, tetragonal, pentagonal, rods and hexagonal shaped gold nanoparticles. The size of the particles was in the range of 8 and 72 nm. The antiproliferative effects of synthesized gold nanoparticles were assessed using C6 glioma human cancer cells. Results indicated that gold nanoparticles synthesized using leaf extracts (150 µg/mL) and stem extracts (200 µg/mL) of P. grandiflora decreased the viability of C6 glioma cell lines up to 50%. © 2016 American Institute of Chemical Engineers Environ Prog, 35: 1732–1740, 2016

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“…The surface morphology of NPs was examined with the JEOL JEM 2100 high-resolution transmission electron microscope. The purity and the chemical composition of the Au NPs were analyzed by EDX spectroscopy an inbuilt of JEOL JEM 2100 (Balasubramani et al 2015a).…”

Section: Characterization Of Gold Nanoparticles (Au Nps)mentioning

confidence: 99%

Lantana camara Linn root extract-mediated gold nanoparticles and their in vitro antioxidant and cytotoxic potentials

Ramkumar¹,

Balasubramani

Raja

et al. 2017

Artificial Cells, Nanomedicine, and Biotechnology

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The Lantana camara Linn root extract derived gold nanoparticles (Au NPs) were characterized by Ultraviolet-Visible spectroscopy, X-ray diffraction, fourier transform-infrared, high resolution transmission electron microscopy, selected area electron diffraction pattern and energy dispersive X-ray analyses. In DPPH assay, the inhibitory concentration (IC) of Au NPs and gallic acid was 24.17 and 5.39 μg/ml, whereas, for cytotoxicity assay, the IC of Au NPs was 17.72 and 32.98 μg/ml on MBA-MB-231 and Vero cells, respectively. Thus, the Au NPs possess significant in vitro antioxidant and cytotoxic properties which could be considered as potential alternate for the development of anticancer drug in future.

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GC–MS analysis of bioactive components and synthesis of gold nanoparticle using Chloroxylon swietenia DC leaf extract and its larvicidal activity

Cited by 48 publications

References 31 publications

Green synthesis and bactericidal activities of isotropic and anisotropic spherical gold nanoparticles produced using Peganum harmala L leaf and seed extracts

Green synthesis and bactericidal activities of isotropic and anisotropic spherical gold nanoparticles produced using Peganum harmala L leaf and seed extracts

Biosynthesis of gold nanoparticles using green roof species Portulaca grandiflora and their cytotoxic effects against C6 glioma human cancer cells

Lantana camara Linn root extract-mediated gold nanoparticles and their in vitro antioxidant and cytotoxic potentials

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