Graphite, an allotropic and stable form of carbon, is a useful material constituted by multiple layers joined with covalent bonds linked together by a weak Van Der Walls interaction. The single units named graphenes have attracted considerable attention, because of their excellent mechanical, chemical, thermal, electrical properties and low thermal expansion coefficient [1]. The strong covalent (sp 2) bonds in this unique honeycomb structure of graphene and their atomic scale thickness impart them with these unusual properties [2]. Taking advantage of the weakness of these interactions, it is possible to insert ions, atoms or molecules between the layers in order to obtain graphenes from graphite. In the exfoliation process, elimination of the intercalated species leads to a significant expansion up to hundreds of times along the c-axis, forming a highly porous material. Exfoliated graphite (EG) has been synthesized by galvanic, chemical and thermal treatments of the natural graphite. However, the chemical method is widely used because its simplicity and versatility. Usually EG is produced intercalating acid guest species between the stacked graphene layers via liquid-phase by reaction between graphite and 18M H 2 SO 4 in the presence of strong chemical oxidants such as KMnO 4 , HNO 3 or H 2 O 2 [3]. However, reaction leftovers are highly toxic and corrosive materials that required careful manipulation and a special confinement.