2021
DOI: 10.1016/j.cogsc.2021.100500
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Green sample preparation methods in the environmental monitoring of aquatic organic pollutants

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Cited by 7 publications
(2 citation statements)
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“…Significant advancements in microwave instrumentation have aided in the synthesis of materials with improved reaction conditions control, producing materials with more desirable physicochemical characteristics. Commercial microwave reactors are now equipped with fiber-optic probes, magnetic stirrers, and sensors for more precise monitoring of the synthesis conditions, resulting in an enhanced reaction yield with higher reproducibility (Favretto, 2003;Ferguson, 2003;Luo et al, 2013b;Dudley et al, 2015), lower energy requirements, and shorter reaction times, among others (Figure 12). However, pressure sensitivity and thresholds (typically lower than 400 psi), and penetration depth limitations are one of the main drawbacks of microwave-assisted synthesis (Antonio De La et al, 2011;de Medeiros et al, 2019).…”
Section: Merits and Challenges Of Microwaveassisted Synthesis Of Carb...mentioning
confidence: 99%
“…Significant advancements in microwave instrumentation have aided in the synthesis of materials with improved reaction conditions control, producing materials with more desirable physicochemical characteristics. Commercial microwave reactors are now equipped with fiber-optic probes, magnetic stirrers, and sensors for more precise monitoring of the synthesis conditions, resulting in an enhanced reaction yield with higher reproducibility (Favretto, 2003;Ferguson, 2003;Luo et al, 2013b;Dudley et al, 2015), lower energy requirements, and shorter reaction times, among others (Figure 12). However, pressure sensitivity and thresholds (typically lower than 400 psi), and penetration depth limitations are one of the main drawbacks of microwave-assisted synthesis (Antonio De La et al, 2011;de Medeiros et al, 2019).…”
Section: Merits and Challenges Of Microwaveassisted Synthesis Of Carb...mentioning
confidence: 99%
“…Sample preparation is an important step in chemical analysis, particularly for trace-level analyte detection, as it can minimize or eliminate matrix interferences, leading to increased sensitivity . Solid-phase microextraction (SPME) , is a commonly used technique for preconcentrating target analytes from complex sample matrixes and has been widely applied in environmental monitoring, food, and pharmaceutical analysis . It involves exposing a sorbent-coated fiber to the sample, followed by thermal or solvent desorption.…”
Section: Introductionmentioning
confidence: 99%