Halothiation as a Method for Oxidation of Primary Halides and Terminal Olefins to Aldehydes

Paquette, Leo A.; Klobucar, W. Dirk; Snow, Robert A.

doi:10.1080/00397917608063551

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Cited by 34 publications

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“…The 1-(chloromethyl)naphthalene was recrystallized from petroleum ether (40-60 °C) until a melting point of 33 °C was obtained. 6-Methylazulene was prepared (28% yield) by a modification of the method of Hafner.9 l-(Thiophenoxymethyl)naphthalene was synthesized by using a slightly modified procedure of Paquette et al 10 The compound had a melting point of 73-73.5 °C (lit.10 mp 72-73.5 °C), and NMR, IR, and MS data consistent with the assigned structure.…”

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confidence: 99%