High-temperature furnace for INEL CPS 120

Muller, Fabrice; Rannou, I.; Duclaux, L.; Guet, J.M.

doi:10.1107/s0021889897004718

Cited by 7 publications

(6 citation statements)

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“…In most cases, such studies are done on powdered samples, often put into capillary sample holders. The use of such capillary sample holders under the Debye-Scherrer diffraction geometry (Guinebretiè re, 2007) together with one-dimensional position-sensitive gaseous (Bé nard et al, 1996;Muller et al, 1997) or solid-state (Pickup et al, 2000;Sarin et al, 2009) curved detectors allows highangular-resolution diffraction patterns to be collected in a short time at temperatures as high as 1250 K. Nevertheless, such an approach is far from the characterization of singlecrystal surfaces, thin films or bulk materials. On the other hand, cylindrical furnaces where platinum foil strips act simultaneously as heating element and sample holder have been under development for many years (Koppelhuber-Bitschnau et al, 1996).…”

Section: Introductionmentioning

confidence: 99%

Full reciprocal-space mapping up to 2000 K under controlled atmosphere: the multipurpose QMAX furnace

et al. 2020

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A furnace that covers the temperature range from room temperature up to 2000 K has been designed, built and implemented on the D2AM beamline at the ESRF. The QMAX furnace is devoted to the full exploration of the reciprocal hemispace located above the sample surface. It is well suited for symmetric and asymmetric 3D reciprocal space mapping. Owing to the hemispherical design of the furnace, 3D grazing-incidence small-and wide-angle scattering and diffraction measurements are possible. Inert and reactive experiments can be performed at atmospheric pressure under controlled gas flux. It is demonstrated that the QMAX furnace allows monitoring of structural phase transitions as well as microstructural evolution at the nanoscale, such as self-organization processes, crystal growth and strain relaxation. A time-resolved in situ oxidation experiment illustrates the capability to probe the high-temperature reactivity of materials. research papers J. Appl. Cryst. (2020). 53, 650-661 René Guinebretière et al. The multipurpose QMAX furnace 651 research papers J. Appl. Cryst. (2020). 53, 650-661 René Guinebretière et al. The multipurpose QMAX furnace 659

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Section: Introductionmentioning

confidence: 99%

Full reciprocal-space mapping up to 2000 K under controlled atmosphere: the multipurpose QMAX furnace

et al. 2020

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“…Variable-temperature X-ray diffraction is important in numerous fields, ranging from mineralogy, the construction of phase diagrams and in situ monitoring of solid-state reactions, to the study of liquid crystals and other organic materials. Many heaters have been described in the past few years, most of which have focused on very high temperature applications, typically reaching temperatures between 1273 and 2273 K (Bellet et al, 2003;Muller et al, 1997;Puig-Molina et al, 2001;Valdrè, 1999). In some cases, the high power consumption required to reach such high temperatures meant that a water cooling system was also necessary (Bellet et al, 2003;Muller et al, 1997).…”

Section: Introductionmentioning

confidence: 99%

“…Many heaters have been described in the past few years, most of which have focused on very high temperature applications, typically reaching temperatures between 1273 and 2273 K (Bellet et al, 2003;Muller et al, 1997;Puig-Molina et al, 2001;Valdrè, 1999). In some cases, the high power consumption required to reach such high temperatures meant that a water cooling system was also necessary (Bellet et al, 2003;Muller et al, 1997). Many of the previously reported furnaces also provide the possibility of operating under controlled atmosphere (Bellet et al, 2003;Puig-Molina et al, 2001;Valdrè, 1999) or offer very high temperature stability (better than AE0.05 K) (Bellet et al, 2003).…”

Section: Introductionmentioning

confidence: 99%

A simple and inexpensive capillary furnace for variable-temperature X-ray diffraction

Lavigueur¹,

Foster²,

Williams³

2008

J Appl Cryst

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An inexpensive capillary furnace has been developed for variable-temperature X-ray diffraction in transmission geometry of air-stable liquid crystals and other materials. It offers temperature control with fluctuations of less than AE1 K in the range of interest for these samples, from room temperature to near 573 K. Phases can be accessed through heating or cooling with no significant overshooting of the target temperature. The furnace is designed to fit on a classical goniometer, and can be controlled by any standard temperature controller. The simple design of this furnace means that it is both inexpensive to build and easy to operate. short communications 216 Christine Lavigueur et al. Capillary furnace J. Appl. Cryst. (2008). 41, 214-216Figure 3(a) X-ray diffraction pattern of compound 3 at 418 K on cooling. (b) Furnace calibration curve.

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“…The furnace must be housed in a cooling jacket, vertically adjustable, so as to optimize the diffraction geometry. More recently, Muller et al (1997), using a similar design, developed a hightemperature furnace that is able to reach 1123 K, with a low temperature gradient along the sample holder capillary; it is designed to work on a curved INEL CPS 120 detector. Again, the furnace is assisted by a cooling system using water circulation.…”

Section: Introductionmentioning

confidence: 99%

An improved low-power-consumption heating stage for X-ray powder diffraction

Valdrè¹

1999

J Appl Cryst

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An improved low-power-consumption easy-to-operate simple heating stage for use in connection with an X-ray powder diffractometer is described and discussed. No modi®cation is required to the conventional specimen chamber, which can be used safely up to a specimen temperature of at least 1200 K with a temperature accuracy of a few degrees. The stage is interchangeable with conventional specimen holders, without the need for realignment of the diffractometer. To prevent specimen oxidation, provisions are made for heating in an inert gaseous environment. Also, care has been taken to prevent scattered radiation escaping from the specimen chamber. The stage allows the study of structural transformations with temperature and so far it has been used successfully for the characterization of very different materials, such as hyaloclastite, smectites, montmorillonites and chlorocadmates with perovskite-like structures. Although the device has been designed for the Philips PW1820 X-ray diffractometer, it can be applied to other types of X-ray diffractometer.

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High-temperature furnace for INEL CPS 120

Cited by 7 publications

References 0 publications

Full reciprocal-space mapping up to 2000 K under controlled atmosphere: the multipurpose QMAX furnace

Full reciprocal-space mapping up to 2000 K under controlled atmosphere: the multipurpose QMAX furnace

A simple and inexpensive capillary furnace for variable-temperature X-ray diffraction

An improved low-power-consumption heating stage for X-ray powder diffraction

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