Hydration reactions and physicochemical properties in a novel tricalcium-dicalcium silicate-based cement containing hydroxyapatite nanoparticles and calcite: A comparative study

Moreno-Vargas, Yoshamin Abnoba; Luna-Arias, Juan Pedro; Flores-Flores, José O.; Orozco, E.; Bucio, L.

doi:10.1016/j.ceramint.2017.07.027

Cited by 13 publications

(13 citation statements)

References 41 publications

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“…Thus far, the effect of HA addition on CSCs has not been studied extensively. However, notably, in a recent study, the addition of 5–15% HA in the form of nanohydroxyapatite (NHA) significantly increased the compressive strength of an experimental CSC [ 30 ]. In contrast, Guerriro-Tanomaru and Vazquez-Garcia reported that the addition of 10–20% NHA reduced the compressive strength and increased the solubility of a CSC-based material [ 31 ].…”

Section: Introductionmentioning

confidence: 99%

Development and Analysis of a Hydroxyapatite Supplemented Calcium Silicate Cement for Endodontic Treatment

et al. 2022

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To develop an endodontic cement using bovine bone-derived hydroxyapatite (BHA), Portland cement (PC), and a radiopacifier. Methods: BHA was manufactured from waste bovine bone and milled to form a powder. The cements were developed by the addition of BHA (10%/20%/30%/40% wt), 35% wt, zirconium oxide (radiopacifier) to Portland cement (PC). A 10% nanohydroxyapatite (NHA) cement containing PC and a radiopacifier, and a cement containing PC (PC65) and a radiopacifier were also manufactured as controls. The cements were characterised to evaluate their compressive strength, setting time, radiopacity, solubility, and pH. The biocompatibility was assessed using Saos-2 cells where ProRoot MTA acted as the control. Compressive strength, solubility and pH were evaluated over a 4-week curing period. Results: The compressive strength (CS) of all cements increased with the extended curing times, with a significant CS increase in all groups from day 1 to day 28. The BHA 10% exhibited significantly higher CS compared with the other cements at all time points investigated. The BHA 10% and 20% groups exhibited significantly longer setting times than BHA 30%, 40% and PC65. The addition of ZrO2 in concentrations above 20% wt and Ta2O5 at 30% wt resulted in a radiopacity equal to, or exceeding that of, ProRoot MTA. The experimental cements exhibited relatively low cytotoxicity, solubility and an alkaline pH. Conclusions: The addition of 10% and 20% BHA to an experimental PC-based cement containing 35% ZrO2 improved the material’s mechanical strength while enabling similar radiopacity and biocompatibility to ProRoot MTA. Although BHA is a cost-effective, biomimetic additive that can improve the properties of calcium silicate endodontic cements, further studies are now warranted to determine its clinical potential.

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Section: Introductionmentioning

confidence: 99%

Development and Analysis of a Hydroxyapatite Supplemented Calcium Silicate Cement for Endodontic Treatment

et al. 2022

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“…Some studies on enhancing the cost-competitive and physical properties of MTA have focused on different particle sizes and compositional manipulations based on ordinary PC at a lower cost and shorter setting time. [6][7][8] Although the most commonly applied radiopacifies for MTA is Bi 2 O 3 , many studies have cited Bi 2 O 3 as the main cause of discoloration in white MTA. [9][10][11] There have been attempts to use a non-Bi 2 O 3 radiopacifying agent (including ZrO 2 , Nb 2 O 5 , and BaZrO 3 ) and especially, ZrO 2 is widely used as radiopacifying instead of Bi 2 O 3 , because of its acceptable radiopacity and color stability.…”

Section: Introductionmentioning

confidence: 99%

Hydration and microhardness of mineral trioxide aggregate depending on ratio between di‐ and tricalcium silicates

Kim

Lee

Rho³

et al. 2021

Int J Applied Ceramic Tech

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Tricalcium silicate (C 3 S) and dicalcium silicate (C 2 S) are the main components related with the hydration process of mineral trioxide aggregates (MTAs) for endodontic materials. In this study, we investigate the influence of different ratios of C 3 S and C 2 S in a series of MTA samples with (100-x)C 3 S-xC 2 S-18ZrO 2 (x = 0, 10, 15, 34, and 100) on their physical and chemical characteristics, hydration process, and microhardness properties. The chemical compositional properties of different samples are measured using X-ray diffraction, X-ray photoelectron spectrometry, and scanning electron microscopy. The physical and microhardness properties are also investigated after the standard hydration process (ISO 6876:2021).Generally, the sample with higher C 3 S ratio induces the faster hydration, which results in decreased fluidity as well as shorter working and setting times. The microhardness generally decreases with larger C 3 S ratio.

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“…MTA has wide dental clinical uses as in cases of; perforation repair, root end filling material, direct and indirect pulp capping, formation of apical plug, and management of immature apices [2, 3]. Its properties include dimensional stability, promotion of cementogenesis, good adhesion to tooth structure, bactericidal properties, inductive of hard tissue formation, and bioactivity [4, 5, 6, 7, 8]. Mineral Trioxide Aggregate that is based on calcium silicate is considered as a hydraulic binder.…”

Section: Introductionmentioning

confidence: 99%

“…Experimentally a highly reactive tri-calcium silicate is prepared in the laboratory at elevated temperatures by solid-state reaction using raw materials unlike those used of Portland cement manufacturing process. Ultra-pure CaO and SiO 2 are used as raw material to avoid contaminations of any impurities as in case of Portland cement production process [8, 22]. This novel single-phase tri-calcium silicate cement preparation aimed to combine the advantages of both MTA and biodentine with lower cost to be used in dental practice.…”

Section: Introductionmentioning

confidence: 99%

Physico-mechanical characteristics of tri-calcium silicate pastes as dentin substitute and interface analysis in class II cavities: effect of CaCl2 and SBF solutions

Radwan

Nagi

El-Hamid

2019

Heliyon

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The influence of using simulated body fluid (SBF) as a curing medium on some characteristics of pure single tri-calcium silicate (C 3 S) bio-cement was investigated. CaCl 2 salt solution was used as an accelerating liquid for setting and hardening of C 3 S pastes in comparison with distilled water (DW). Solid state reaction was applied to synthesis C 3 S phase at elevated temperature followed by rapid cooling. The results showed that 10 wt.% CaCl 2 solution was the optimum concentration that showed the lowest setting time (106 min). C 3 S pastes prepared with CaCl 2 solution have better physical and mechanical properties than those mixed with DW even after curing under SBF solution for the different curing ages. However, SBF solution has an adverse effect on the hydrated compound C-S-H that results in a little decrease in strength and hardness values. The elemental analysis emphasized the presence of apatite layer on the surface of the hardened C 3 S paste. Scanning electron microscopy (SEM) photomicrographs and elemental analysis revealed reliable adaptation of the experimentally prepared C 3 S paste to the tooth structure, in addition to its bioactivity makes it a consistent material to be used as dentin substitute.

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Hydration reactions and physicochemical properties in a novel tricalcium-dicalcium silicate-based cement containing hydroxyapatite nanoparticles and calcite: A comparative study

Cited by 13 publications

References 41 publications

Development and Analysis of a Hydroxyapatite Supplemented Calcium Silicate Cement for Endodontic Treatment

Development and Analysis of a Hydroxyapatite Supplemented Calcium Silicate Cement for Endodontic Treatment

Hydration and microhardness of mineral trioxide aggregate depending on ratio between di‐ and tricalcium silicates

Physico-mechanical characteristics of tri-calcium silicate pastes as dentin substitute and interface analysis in class II cavities: effect of CaCl2 and SBF solutions

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