“…N2-H1N2Á Á ÁO1 and C17-H17Á Á ÁO2, forming a five-and six-membered ring, respectively. The crystal packing is stabilized by intermolecular N2-H1N2Á Á ÁO1W, C13-H13Á Á ÁO1W and O1W-H1W1Á Á ÁN1 hydrogen bonds (Table 2 and Experimental 2-Chloro-N-phenylacetamide was prepared by the reaction of phenylamine and chloroacetyl chloride in the presence of triethylamine, according to the literature method of Wen et al (2004). To a solution of 8-hydroxyquinoline (1.45 g, 10 mmol) in acetone (40 ml) were added 2-chloro-N-phenylacetamide (1.69 g, 10 mmol), K 2 CO 3 (1.52 g, 11 mmol) and KI (0.5 g), and the resulting mixture was stirred at 333 K for 5 h. After cooling to room temperature, the mixture was washed three times with water and then filtered.…”