In situ analysis of electrocrystallization process of metal electrodeposition with confocal energy dispersive X-ray diffraction based on polycapillary X-ray optics

Li, Fangzuo; Liu, Zhiguo; Sun, Tao; Yang, Chaolin; Sun, Weiyuan; Sun, Xuepeng; Ma, Yongzhong; Ding, Xunliang

doi:10.1016/j.nima.2015.03.015

Cited by 8 publications

(4 citation statements)

References 36 publications

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“…This confocal micro-EDXRD spectrometer can also be used for the phase and structure formation investigation of metal electrocrystallization nucleation and growth. The experimental results demonstrate the possibilities of the in situ and time-resolved analysis of the electrocrystalization process of metal electrodeposition by laboratory confocal EDXRD (Li et al 2015b).…”

Section: Experimental Design and Applications Of Confocal Xrdmentioning

confidence: 57%

Confocal X-ray technology based on capillary X-ray optics

Sun¹,

Ding²

2015

Reviews in Analytical Chemistry

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Capillary X-ray optics is versatile, and it can be used with synchrotron radiation source, conventional X-ray source, laser-plasma ultrafast X-ray source, and so forth. Recently, the confocal X-ray technology based on capillary X-ray optics has become popular, and it has been widely used in X-ray fluorescence, X-ray absorption fine structure, X-ray diffraction, small-angle X-ray scattering, X-ray imaging, and X-ray scattering. This confocal X-ray technology has applications in many fields, including environmental monitoring, food science, life science, chemistry, physics, nanomaterials, nondestructive test, security check, and so on.

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Section: Experimental Design and Applications Of Confocal Xrdmentioning

confidence: 57%

Confocal X-ray technology based on capillary X-ray optics

Sun¹,

Ding²

2015

Reviews in Analytical Chemistry

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“…ions from the electrolyte to the electrode surface and deposited, following the atom being placed into the crystal lattice and growth [51]. This concord with the law of cathodic reduction of aqueous solution and the fundamental law of crystallization processing, but somehow complicated to the kinetic law of cathodic reduction because the electrode attracts particles continuously.…”

Section: Mechanismmentioning

confidence: 96%

Superhydrophobic Coating Fabrication for Metal Protection Based on Electrodeposition Application: A Review

Miller¹,

Hu²,

Weamie³

et al. 2021

MSCE

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In recent years, superhydrophobic media has attracted tremendous attention due to its industrial applicability value, especially in anti-corrosion performance. The superhydrophobic coating, which has a robust and water-repellent capacity, can catch the air to form several "airbags" on the substrate's surface, isolating the corrosion media. Various superhydrophobic coating preparation technologies have been suggested, but each has its own set of flaws. On the other hand, electrodeposition, as a relatively mature industrial processing application, offers distinct advantages. However, until now, there have been few reviews on the electrodeposition preparation of anticorrosive superhydrophobic coatings. Therefore, the author has described several fabrication techniques based on superhydrophobic coatings in this review, including the advantages and disadvantages. Superhydrophobic coatings conventional concepts and wettability, as well as the model wetting concepts, have been reviewed. The coating processing status and the corrosion-resistant potential through the electrodeposition of metal and comparable composite are detailly encapsulated. Furthermore, electrodeposition parameters, including current density, crystal modifiers, and a deposition time of the coating morphology, are reported, following the ultrasonic-assisted, jet, pulse, and magnetic field-induced electrodeposition, respectively, as the recently developed technologies for preparing a coating. Finally, technology limitation is shown as well as the obstacles and prospects, and the improvement of the superhydrophobic coating's durability as a prospects research focus has been recommended.

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“…Comparison of microstress measurements showed a marked reduction in uncertainty with polycapillary optics (110). A system using confocal geometry was designed for scanning diffractometry for in situ measurement of thin-film deposition (111) to measure grain sizes (112). In addition, replacing a Soller slit with a polycapillary straight angular filter (113) provided an approximately factor-of-two gain in signal-to-noise ratio for the identification of the ξ phase on a galvannealed steel sheet (114).…”

Section: Diffractionmentioning

confidence: 99%

Structured X-Ray Optics for Laboratory-Based Materials Analysis

MacDonald

2017

Annu. Rev. Mater. Res.

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Metamaterials provide a challenge for materials analysis, as large-scale 3D geometries confound traditional methods. X-ray optics that allow for novel beam geometries and for more efficient use of conventional X-ray sources can be important in defect and structure analysis to close the loop between design and performance. Fortunately, metamaterials have also provided a new variety of array and structured X-ray optics. Because X-rays barely interact with materials, their index of refraction in any material is only slightly different from unity, so it is very difficult to make the sort of refractive optics that are used for visible light. Instead, diffraction can be used to control the direction or wavelength of X-rays. Structured diffractive optics include transmission gratings, artificial multilayers, and arrays of curved crystals. X-rays also have very high reflectivity at grazing incidence. This phenomenon allows for reflective arrays such as multipore and polycapillary optics.

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In situ analysis of electrocrystallization process of metal electrodeposition with confocal energy dispersive X-ray diffraction based on polycapillary X-ray optics

Cited by 8 publications

References 36 publications

Confocal X-ray technology based on capillary X-ray optics

Confocal X-ray technology based on capillary X-ray optics

Superhydrophobic Coating Fabrication for Metal Protection Based on Electrodeposition Application: A Review

Structured X-Ray Optics for Laboratory-Based Materials Analysis

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