Influence of a polycrystalline precipitation zone on the growth of single crystals using a gel method: growth of single crystals of PbHPO4

Mayer, K.; Woermann, D.

doi:10.1016/s0022-0248(96)00398-3

Cited by 5 publications

(1 citation statement)

References 16 publications

Supporting

Mentioning

Contrasting

Order By: Relevance

“…But sparingly insoluble inorganic substances cannot be grown easily by solution or melt growth techniques. One of the possibilities to grow single crystals of sparingly insoluble inorganic substance is the use of gel method [6][7][8][9]. In this present work, single crystals of zinc hydrogen phosphate (ZnHPO 4 ) are grown successfully using sodium meta silicate gel [10][11][12][13].…”

Section: Introductionmentioning

confidence: 99%

Growth and characterization of nonlinear optical zinc hydrogen phosphate single crystal grown in silica gel

Raj¹,

Mangalam

Priya³

et al. 2007

Cryst. Res. Technol.

View full text Add to dashboard Cite

Good optical quality single crystals of zinc hydrogen phosphate (ZnHPO 4 ) having dimensions up to 8×2×2 mm 3 have been grown with the aid of sodium meta silicate gel. Single crystal XRD studies confirm that the crystal belongs to the orthorhombic system with space group P2 1 2 1 2 1 . The functional groups present in the crystals were confirmed using FTIR technique. Optical absorbance shows very low absorption in the entire visible region. Differential thermal and thermo gravimetric analysis confirmed that the crystal is stable up to 193°C. Photoconductivity study reveals positive photoconductivity in the presence of photo active centers formed by trap energy levels. The NLO activity of the crystal was confirmed by Kurtz powder technique.

show abstract

Section: Introductionmentioning

confidence: 99%

Growth and characterization of nonlinear optical zinc hydrogen phosphate single crystal grown in silica gel

Raj¹,

Mangalam

Priya³

et al. 2007

Cryst. Res. Technol.

View full text Add to dashboard Cite

show abstract

Crystallization from Gels

Kalkura

Natarajan

2010

Springer Handbook of Crystal Growth

View full text Add to dashboard Cite

dia 32 1997 4 569-575Crystallization of an organic intercalation compound : cholic acid Crystals of cholic acid have been grown in silica and tetramethoxy silane gels. Crystals grew with different morphology and Leisegang rings were also seen in mme cases. Crystals were analyzed by X-ray, IR and microhardness studies. The grown crystals were found to be monohydrate and the hardness of the crystals were found to decrease with increase of load.

show abstract