Influence of Nickel Powder Particle Size on the Microstructure and Densification of Spark Plasma Sintered Nickel-Based Superalloy

Abstract

This study aims to investigate the effects of powder particle size on the densification and microhardness properties of spark plasma sintered superalloy. Three particles size ranges of nickel were used in this study, namely, (3-44, 45-106 and 106-150 μm), and this is the matrix in the IN738LC superalloy composition (powder), used in the study. The effects of the particle size were examined at a specific applied temperature and pressure. The transitioning stages during the sintering process of the green powders to the formation of the sintered alloy were analyzed and given as the particle rearrangement stage, the localized deformation stage and the neck formation/grain growth stage. There was the formation of γ, γ' and a solid solution within the microstructure of the sintered alloys. The effect of particle size was more pronounced on the grain sizes obtained, while the phases formed is the same for the three alloys. The results indicate that the nickel particle size (>60% of the total composition) has a significant influence on the densification, porosity, grain size and hardness properties of the IN738LC sintered alloy. Finer nickel particle size resulted in a sintered product with smaller grain size (9 µm), reduced percentage porosity (3.9%), increased relative density (96.1%) and increased hardness properties (371 Hv).

The effects of sintering additives on the ceramic matrix composite of ZrO2: microstructure, densification, and mechanical properties – a review

“…The generated plasma influences the increasing temperature, although the growth of the necks which resultantly promotes an increase in the mass movement is initiated by melting that happens at the contact point of the particles' surface of the powder [28]. Morita et al and Xie et al all stated that the quickening effects of plasma will eliminate the carbon in the graphite sheets and the gaseous carbon would decrease the powder's surface oxide, which gave additional plausible influence of plasma [31][32][33]. Zhang et al [34] elucidate that due to the discharge of plasma between the die and punch during the sintering process, that the ejection of spark intensifies the thermal diffusion of the materials [35][36][37].…”