The melt thermo-temporal processing technology of using the results of analysis, which allowed to recommend it in the production of large-tonnage ingots and amorphous materials on iron, nickel and aluminum bases, was carried out. Thermo-temporal treatment of the melt leads to a favorable structure formation, decrease in its chemical and physical heterogeneity, reduction in size and number of shrinkage defects. These usually are accompanied by an increase in technological and service characteristics of alloys. The usable products suitable alloy increases, the metal consumption of products decreases.