This work presents the results of experimental laboratory tests on the apodization of circular and rectangular apertures using the Interferometric Apodization by Homothety (IAH) technique. The IAH approach involves splitting the amplitude of the instrumental PSF into two equal parts. One of the two produced PSFs undergoes homothety to change its transverse dimensions while its amplitude is properly controlled. The two PSFs are then combined to produce an apodized image. The diffraction wings of the resulting PSF are subsequently reduced by some variable reduction factor, depending on an amplitude parameter γ and a spread parameter η. This apodization approach was implemented in the laboratory using an interferometric set-up based on the Mach–Zehnder Interferometer (MZI). The experimental results exhibit a strong agreement between theory and experiment. For instance, the average experimental contrast obtained at a low angular separation of 2.4λ/D does not exceed 5 × 10−4. This work also allowed us to study the influence on the apodizer’s performance of some parameters, such as the wavelength and the density of the neutral filters.