Investigation of the chiral recognition role of cyclodextrin hydroxyl moieties <i>via</i> high performance liquid chromatography

Li, Yuan; Jin, Xiaoning; Xiao, Yin; Ma, Xiaofei; Wang, Yong

doi:10.1039/d3an01033c

Analyst

2023

DOI: 10.1039/d3an01033c

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Investigation of the chiral recognition role of cyclodextrin hydroxyl moieties via high performance liquid chromatography

Yuan Li,

Xiaoning Jin,

Yin Xiao

et al.

Abstract: Cyclodextrin (CD) is known to afford excellent enantioselectivities due to its hydrophobic cavity and external H-bonding sites from hydroxyl moieties. However, there is still lack of direct and comprehensive evidences...

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Polysaccharide materials have wide applications in the field of chiral recognition. Herein, a new series of chiral materials based on chiral polysaccharide were synthesized for electrochemical enantioselective recognition of tryptophan (Trp) enantiomers. Chiral recognition was investigated via differential pulse voltammetry (DPV). Among poly (L‐lactide) La/hydroxyapatite chitosan (PLLHC‐X) series materials (PLLHC‐0, PLLHC‐1, PLLHC‐3, PLLHC‐7 PLLHC‐9 and PLLHC‐5), PLLHC‐5 has the best recognition efficiency. And the results reveal that the PLLHC‐5 displays a stronger interaction with L‐Trp than to that of D‐Trp. The synergetic effect of chiral recognition from chitosan and signal amplification from poly (L‐la

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Recent advances in application of cyclodextrin-based chiral materials for enantioseparation

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Investigation of the chiral recognition role of cyclodextrin hydroxyl moieties via high performance liquid chromatography

Abstract: Cyclodextrin (CD) is known to afford excellent enantioselectivities due to its hydrophobic cavity and external H-bonding sites from hydroxyl moieties. However, there is still lack of direct and comprehensive evidences...

Cited by 3 publications

References 36 publications

Chiral Electrochemical Sensing Platform Constructed by Chiral Chitosan Materials for Enhanced Electrochemical Chiral Analysis

Chiral Electrochemical Sensing Platform Constructed by Chiral Chitosan Materials for Enhanced Electrochemical Chiral Analysis

Recent advances in application of cyclodextrin-based chiral materials for enantioseparation

β-Cyclodextrin modified imidazole probe specific recognition of organic acids based on nuclear magnetic resonance

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