Nanostructured nickel coatings with molybdenum disulphide particles were electrodeposited to form composite coatings. Three different current densities, i.e. 3, 5 and 7 A/dm 2 were investigated initially. The best results were obtained with 5 A/dm 2 for codeposition of nanostructured Ni-MoS 2 composite coatings. With the addition of 1-4 g/L molybdenum disulphide to the bath, the weight percentages of MoS 2 particles in the coatings were 23-38%. This increase of MoS 2 content was accompanied with decrease in friction coefficient of the coatings from 0.35 to 0.08. Wear resistance of the coatings was increased with increasing MoS 2 content and the weight loss was decreased from 1.4 to 0.7 mg. Hardness was decreased from 585 to 400 VHN with increasing the MoS 2 content. By increasing bath agitation speed up to 150 rpm, more MoS 2 particles were embedded in the matrix and the coatings showed better wear resistance. However, increase of agitation speed from 150 to 200 rpm caused a decrease of MoS 2 particles in the nickel matrix due to the turbulent motion of particles in the bath. Overall, it was shown that the lubricating effect of MoS 2 in the coating was more influential than the nanocrystallinity of the nickel matrix in improving tribological properties of these composite coatings.