Large-scale synthesis of ultralong Sb2S3 sub-microwires via a hydrothermal process

Preparation and characterization of the rod-shaped stibnite

“…We note the appearance of (1 0 2), (2 0 2) and (1 0 3) peaks corresponding to the most intense orientations which are characteristic of the orthorhombic phase. These are in agreement with those found in the literature [7,11]. It is also worth noting that no other phases are detected by means of XRD analysis indicating a high purity of obtained film.…”

“…These films are used in various applications, as principal elements in optoelectronic and photovoltaic devices and exhibit hydrophobic properties [4][5][6]. A range of nanostructures Sb 2 S 3 with different morphologies and architectures have been prepared by several techniques such as hydrothermal process, solvothermal route, hydrolysis and microwave-assisted heating methods [7][8][9][10]. On the other hand, Sb 2 S 3 has an orthorhombic lattice-shaped structure consisting from infinite atom chains or chain of (Sb x S y ).…”

One-Dimensional Rod-Like Sb2S3-Based Anode for High-Performance Sodium-Ion Batteries

“…On the basis of some previous laudable works, − the possible formation process of the Sb 2 S 3 rods is depicted in Scheme . When the thiourea solution was added into the SbCl 3 solution, a Sb-thiourea complex was formed.…”

Hydrothermal synthesis of double sheaf-like Sb2S3 using copolymer as a crystal splitting agent

“…Its property is generally controlled by the morphologies with different defects and concentrations. A number of methods have been used to synthesize antimony sulfide with different morphologies: nanocrystals by a microwave synthesis [3], dendrites by the crystallization of amorphous colloidal microspheres [4], and straw-tied-like architectures, nanoribbons and sub-microwires by a hydrothermal process [1,5,6].…”