2022
DOI: 10.2109/jcersj2.21146
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Liquid-phase synthesis of advanced ceramic sorbents with high functionalization and morphological control

Abstract: Sorption properties, induced by surface reaction such as adsorption, absorption, and ion-exchange reactions, of ceramics are affected by crystallographic properties, including crystallinity, structure, size, and morphology. Through the hydrothermal process, which is a part of the liquid-phase synthesis, crystals with various morphologies can be synthesized in a relatively short time and at low temperatures. Therefore, this process is an effective technique for the enhancement of sorption properties as it facil… Show more

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Cited by 4 publications
(6 citation statements)
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“…Collectively, the XRD patterns, SEM images, and particle size distributions (Figs. 24) reveal that the increase in the crystal size in the GAC-GC-Hs is proportional to the amount of both WO 3 and carbon. Given the lack of a substantial difference in the volume fractions and an increase in the size of bright spots between Products A and B (Fig.…”
Section: Formation Of Cas Gc-h With Relatively Coarse Microstructure ...mentioning
confidence: 96%
“…Collectively, the XRD patterns, SEM images, and particle size distributions (Figs. 24) reveal that the increase in the crystal size in the GAC-GC-Hs is proportional to the amount of both WO 3 and carbon. Given the lack of a substantial difference in the volume fractions and an increase in the size of bright spots between Products A and B (Fig.…”
Section: Formation Of Cas Gc-h With Relatively Coarse Microstructure ...mentioning
confidence: 96%
“…For instance, solvent control or reactivity of raw materials with water results in large morphological changes. 13,14 The controlled release of water in the solvent is estimated to have a significant effect on HAp formation under hydrothermal or solvothermal conditions. However, the crystal growth behaviour of HAp in an environment with extremely limited water in the organic solvent has not been reported extensively.…”
Section: Introductionmentioning
confidence: 99%
“…11 The morphology and composition of HAp are also easily altered in the hydrothermal method via starting materials and treatment conditions such as temperature, solvents, and additives. 6,[9][10][11][12][13] In general, nucleation and crystal growth behaviour in the liquid phase is strongly affected by the supersaturation degree and its change rate. In addition, the presence of 'water' in the liquid phase is key for the nucleation and crystal growth of HAp, and the contribution of water is particularly large on HAp formation, as can be also inferred from the chemical composition.…”
Section: Introductionmentioning
confidence: 99%
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“…2) In addition, the availability of a wide range of chemical reactions and physical phenomena of liquid-phase synthesis is suitable for controlling the morphological and structural properties of ceramic powders consisting of nano-, micro-, and macrosized crystals. 1,3) Such control of morphology and structure is extremely important because it is well known that functionality of inorganic materials is strongly dependent on their chemical composition, particle morphology, size, and so on. 4) Indeed, many reviews are being published even recently on morphology and structure control using liquid phase synthesis for various materials such as metal oxides, 2,4) layered double hydroxides 5) and lithium-ion battery cathode materials.…”
Section: Introductionmentioning
confidence: 99%